data_pop5 _audit_update_record ; 2021-11-21 # Formatted by publCIF ; _publcif_datablock.id '{d105f0f2-f86b-4b6f-87d0-438749181ddb}' # publcif _publ_body_element loop start loop_ _publ_body_element _publ_body_title _publ_body_contents section ; Chemical context ; ; ; section ; Structural commentary ; ; ; section ; Supramolecular features ; ; ; section ; Database survey ; ; ; section ; Synthesis and crystallization ; ; ; section ; Refinement ; ; Crystal data, data collection and structure refinement details are summarized in Table 1. ; # publcif _publ_body_element loop end # start Validation Reply Form _vrf_PLAT220_pop5 ; PROBLEM: NonSolvent Resd 1 C Ueq(max)/Ueq(min) Range 7.5 Ratio RESPONSE: All the atoms are assigned correctly. ; # end Validation Reply Form _audit_creation_method 'SHELXL-2018/3' _shelx_SHELXL_version_number '2018/3' _chemical_name_systematic ? _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety ? _chemical_formula_sum 'C40.90 H65.70 Fe N2 O Si' _chemical_formula_weight 685.38 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Fe' 'Fe' -1.1336 3.1974 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Si' 'Si' 0.2541 0.3302 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_H-M_alt 'P 21/n' _space_group_name_Hall '-P 2yn' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' _cell_length_a 13.0003(2) _cell_length_b 21.8240(4) _cell_length_c 16.1198(3) _cell_angle_alpha 90 _cell_angle_beta 113.1150(10) _cell_angle_gamma 90 _cell_volume 4206.32(13) _cell_formula_units_Z 4 _cell_measurement_temperature 100(2) _cell_measurement_reflns_used 9823 _cell_measurement_theta_min 3.60 _cell_measurement_theta_max 66.55 _exptl_crystal_description 'block' _exptl_crystal_colour 'red' _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 1.082 _exptl_crystal_F_000 1492 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.241 _exptl_crystal_size_mid 0.209 _exptl_crystal_size_min 0.122 _exptl_absorpt_coefficient_mu 3.361 _shelx_estimated_absorpt_T_min 0.498 _shelx_estimated_absorpt_T_max 0.685 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_min 0.5583 _exptl_absorpt_correction_T_max 0.7528 _exptl_absorpt_process_details 'TWINABS BRUKER AXS' _exptl_absorpt_special_details ? _diffrn_ambient_temperature 100(2) _diffrn_radiation_wavelength 1.54178 _diffrn_radiation_type CuK\a _diffrn_source ? _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_detector_area_resol_mean ? _diffrn_reflns_number 83388 _diffrn_reflns_av_unetI/netI 0.0358 _diffrn_reflns_av_R_equivalents 0.0881 _diffrn_reflns_limit_h_min -15 _diffrn_reflns_limit_h_max 15 _diffrn_reflns_limit_k_min -25 _diffrn_reflns_limit_k_max 24 _diffrn_reflns_limit_l_min -19 _diffrn_reflns_limit_l_max 19 _diffrn_reflns_theta_min 3.604 _diffrn_reflns_theta_max 66.736 _diffrn_reflns_theta_full 66.736 _diffrn_measured_fraction_theta_max 0.998 _diffrn_measured_fraction_theta_full 0.998 _diffrn_reflns_Laue_measured_fraction_max 0.998 _diffrn_reflns_Laue_measured_fraction_full 0.998 _diffrn_reflns_point_group_measured_fraction_max 0.998 _diffrn_reflns_point_group_measured_fraction_full 0.998 _reflns_number_total 7459 _reflns_number_gt 5819 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection 'Bruker APEX2' _computing_cell_refinement 'Bruker SAINT' _computing_data_reduction 'Bruker SAINT' _computing_structure_solution 'SHELXS-97 (Sheldrick 2008)' _computing_structure_refinement 'SHELXL-2014 (Sheldrick 2014)' _computing_molecular_graphics 'Bruker SHELXTL' _computing_publication_material 'Bruker SHELXTL' _refine_special_details ? _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0699P)^2^+3.7468P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_number_reflns 7459 _refine_ls_number_parameters 448 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0722 _refine_ls_R_factor_gt 0.0523 _refine_ls_wR_factor_ref 0.1437 _refine_ls_wR_factor_gt 0.1301 _refine_ls_goodness_of_fit_ref 1.037 _refine_ls_restrained_S_all 1.037 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group C1 C 0.2965(3) 0.63648(14) 0.61605(18) 0.0376(7) Uani 1 1 d . . . . . H1A H 0.376179 0.633569 0.651939 0.045 Uiso 1 1 calc R U . A 1 H1B H 0.268780 0.672543 0.635806 0.045 Uiso 1 1 calc R U . A 1 C5 C 0.4260(2) 0.64502(11) 0.38595(17) 0.0247(6) Uani 1 1 d . . . . . H5 H 0.494178 0.654812 0.383222 0.030 Uiso 1 1 calc R U . . . C6 C 0.3495(2) 0.61014(11) 0.31122(16) 0.0228(5) Uani 1 1 d . . . . . C7 C 0.2448(2) 0.58884(11) 0.30730(16) 0.0227(5) Uani 1 1 d . . . . . C8 C 0.1738(2) 0.55666(11) 0.22772(17) 0.0232(5) Uani 1 1 d . . . . . C9 C 0.2126(2) 0.54753(11) 0.15991(17) 0.0242(6) Uani 1 1 d . . . . . H9 H 0.165983 0.527155 0.108123 0.029 Uiso 1 1 calc R U . . . C10 C 0.3182(2) 0.56703(12) 0.16399(17) 0.0249(6) Uani 1 1 d . . . . . C11 C 0.3844(2) 0.59786(11) 0.24024(17) 0.0254(6) Uani 1 1 d . . . . . H11 H 0.454696 0.611149 0.245498 0.031 Uiso 1 1 calc R U . . . C12 C 0.0591(2) 0.53254(12) 0.21939(17) 0.0267(6) Uani 1 1 d . . . . . C13 C 0.0742(2) 0.48491(14) 0.29321(19) 0.0340(7) Uani 1 1 d . . . . . H13A H 0.116611 0.450859 0.285819 0.051 Uiso 1 1 calc R U . . . H13B H 0.002235 0.470863 0.288686 0.051 Uiso 1 1 calc R U . . . H13C H 0.113298 0.503188 0.351348 0.051 Uiso 1 1 calc R U . . . C14 C -0.0156(2) 0.58536(14) 0.2265(2) 0.0354(7) Uani 1 1 d . . . . . H14A H 0.016330 0.602872 0.285869 0.053 Uiso 1 1 calc R U . . . H14B H -0.088967 0.569908 0.215570 0.053 Uiso 1 1 calc R U . . . H14C H -0.020823 0.616202 0.182603 0.053 Uiso 1 1 calc R U . . . C15 C -0.0040(2) 0.50070(14) 0.12855(18) 0.0332(6) Uani 1 1 d . . . . . H15A H -0.015365 0.529194 0.080368 0.050 Uiso 1 1 calc R U . . . H15B H -0.075159 0.486525 0.125886 0.050 Uiso 1 1 calc R U . . . H15C H 0.038968 0.466484 0.122578 0.050 Uiso 1 1 calc R U . . . C16 C 0.3525(2) 0.55469(13) 0.08457(18) 0.0309(6) Uani 1 1 d . . . . . C17 C 0.3358(3) 0.48667(14) 0.0581(2) 0.0449(8) Uani 1 1 d . . . . . H17A H 0.382791 0.462099 0.108018 0.067 Uiso 1 1 calc R U . . . H17B H 0.355278 0.479752 0.007273 0.067 Uiso 1 1 calc R U . . . H17C H 0.258994 0.475651 0.042566 0.067 Uiso 1 1 calc R U . . . C18 C 0.2788(3) 0.59384(15) 0.0041(2) 0.0430(8) Uani 1 1 d . . . . . H18A H 0.201623 0.583449 -0.011701 0.065 Uiso 1 1 calc R U . . . H18B H 0.298549 0.586150 -0.046403 0.065 Uiso 1 1 calc R U . . . H18C H 0.290036 0.636419 0.020085 0.065 Uiso 1 1 calc R U . . . C19 C 0.4748(3) 0.57156(17) 0.1077(2) 0.0473(8) Uani 1 1 d . . . . . H19A H 0.485570 0.614453 0.121659 0.071 Uiso 1 1 calc R U . . . H19B H 0.493748 0.562716 0.057056 0.071 Uiso 1 1 calc R U . . . H19C H 0.522010 0.548111 0.158888 0.071 Uiso 1 1 calc R U . . . C20 C 0.5005(2) 0.69923(13) 0.52065(17) 0.0283(6) Uani 1 1 d . . . . . C21 C 0.5787(3) 0.66866(15) 0.5956(2) 0.0400(7) Uani 1 1 d . . . . . C22 C 0.6637(3) 0.70394(18) 0.6574(2) 0.0521(9) Uani 1 1 d . . . . . H22 H 0.717049 0.685117 0.707647 0.063 Uiso 1 1 calc R U . . . C23 C 0.6703(3) 0.76664(18) 0.6455(2) 0.0517(9) Uani 1 1 d . . . . . H23 H 0.728405 0.789155 0.687201 0.062 Uiso 1 1 calc R U . . . C24 C 0.5914(3) 0.79552(15) 0.5725(2) 0.0409(7) Uani 1 1 d . . . . . H24 H 0.596110 0.837613 0.565701 0.049 Uiso 1 1 calc R U . . . C25 C 0.5045(2) 0.76260(13) 0.50851(18) 0.0305(6) Uani 1 1 d . . . . . C26 C 0.5720(3) 0.59983(16) 0.6058(2) 0.0510(9) Uani 1 1 d . . . . . H26 H 0.492860 0.588377 0.578207 0.061 Uiso 1 1 calc R U . . . C27 C 0.6316(3) 0.56573(18) 0.5559(2) 0.0644(11) Uani 1 1 d . . . . . H27A H 0.596115 0.574607 0.492618 0.097 Uiso 1 1 calc R U . . . H27B H 0.628045 0.522478 0.565305 0.097 Uiso 1 1 calc R U . . . H27C H 0.708384 0.578475 0.578121 0.097 Uiso 1 1 calc R U . . . C28 C 0.6168(3) 0.57857(19) 0.7043(3) 0.0627(11) Uani 1 1 d . . . . . H28A H 0.696280 0.584795 0.731430 0.094 Uiso 1 1 calc R U . . . H28B H 0.600604 0.535840 0.706491 0.094 Uiso 1 1 calc R U . . . H28C H 0.581734 0.601757 0.736539 0.094 Uiso 1 1 calc R U . . . C29 C 0.4198(3) 0.79502(13) 0.42691(19) 0.0346(7) Uani 1 1 d . . . . . H29 H 0.358641 0.766196 0.396716 0.042 Uiso 1 1 calc R U . . . C30 C 0.3693(3) 0.85160(14) 0.4526(3) 0.0517(9) Uani 1 1 d . . . . . H30A H 0.336790 0.840098 0.494489 0.078 Uiso 1 1 calc R U . . . H30B H 0.312511 0.868696 0.399427 0.078 Uiso 1 1 calc R U . . . H30C H 0.426843 0.881510 0.479956 0.078 Uiso 1 1 calc R U . . . C31 C 0.4718(3) 0.81200(15) 0.3599(2) 0.0452(8) Uani 1 1 d . . . . . H31A H 0.534274 0.838815 0.388621 0.068 Uiso 1 1 calc R U . . . H31B H 0.417007 0.832367 0.308880 0.068 Uiso 1 1 calc R U . . . H31C H 0.496686 0.775500 0.340215 0.068 Uiso 1 1 calc R U . . . C32 C 0.1388(3) 0.76337(16) 0.4856(2) 0.0510(9) Uani 1 1 d . . . . . H32 H 0.175876 0.759240 0.547725 0.061 Uiso 1 1 calc R U . . . C33 C 0.0623(4) 0.81029(19) 0.4523(3) 0.0690(12) Uani 1 1 d . . . . . H33 H 0.049705 0.837558 0.491656 0.083 Uiso 1 1 calc R U . . . C34 C 0.0054(4) 0.81645(19) 0.3616(3) 0.0692(12) Uani 1 1 d . . . . . H34 H -0.047559 0.847299 0.338286 0.083 Uiso 1 1 calc R U . . . C35 C 0.0275(3) 0.77651(17) 0.3056(3) 0.0563(10) Uani 1 1 d . . . . . H35 H -0.009750 0.779905 0.243323 0.068 Uiso 1 1 calc R U . . . C36 C 0.1058(3) 0.73107(14) 0.3426(2) 0.0419(7) Uani 1 1 d . . . . . H36 H 0.120723 0.704287 0.303862 0.050 Uiso 1 1 calc R U . . . C37 C 0.9028(7) 0.7167(4) 0.5801(5) 0.138(3) Uani 1 1 d . . . . . H37A H 0.966549 0.691627 0.587729 0.207 Uiso 1 1 calc R U . . . H37B H 0.879614 0.709322 0.628950 0.207 Uiso 1 1 calc R U . . . H37C H 0.922292 0.759090 0.579886 0.207 Uiso 1 1 calc R U . . . C38 C 0.8117(7) 0.7016(6) 0.4950(5) 0.198(5) Uani 1 1 d . . . . . H38A H 0.788581 0.660609 0.503713 0.237 Uiso 1 1 calc R U . . . H38B H 0.750841 0.728426 0.491952 0.237 Uiso 1 1 calc R U . . . O2 O 0.8095(6) 0.7013(4) 0.4101(4) 0.207(3) Uani 1 1 d . . . . . C40 C 0.7240(5) 0.6912(4) 0.3252(4) 0.122(2) Uani 1 1 d . . . . . H40A H 0.665755 0.720214 0.321304 0.147 Uiso 1 1 calc R U . . . H40B H 0.694350 0.651038 0.329279 0.147 Uiso 1 1 calc R U . . . C41 C 0.7291(6) 0.6926(5) 0.2407(4) 0.196(5) Uani 1 1 d . . . . . H41A H 0.805387 0.687979 0.247381 0.293 Uiso 1 1 calc R U . . . H41B H 0.700411 0.730985 0.211959 0.293 Uiso 1 1 calc R U . . . H41C H 0.685054 0.659672 0.204516 0.293 Uiso 1 1 calc R U . . . Fe1 Fe 0.27137(4) 0.64721(2) 0.48207(3) 0.02699(14) Uani 1 1 d . . . . . N1 N 0.41116(18) 0.66432(10) 0.45623(14) 0.0251(5) Uani 1 1 d . . . . . N2 N 0.1616(2) 0.72349(11) 0.43174(16) 0.0330(5) Uani 1 1 d . . . . . O1 O 0.21201(15) 0.59822(8) 0.37376(12) 0.0271(4) Uani 1 1 d . . . . . C2 C 0.0781(6) 0.5708(6) 0.5617(4) 0.170(5) Uani 0.897(6) 1 d . . P B 1 H2A H 0.070259 0.574604 0.500206 0.255 Uiso 0.897(6) 1 calc R U P B 1 H2B H 0.042938 0.605123 0.577230 0.255 Uiso 0.897(6) 1 calc R U P B 1 H2C H 0.043126 0.533561 0.568850 0.255 Uiso 0.897(6) 1 calc R U P B 1 C3 C 0.2459(4) 0.5611(3) 0.7580(3) 0.0623(15) Uani 0.897(6) 1 d . . P B 1 H3A H 0.214148 0.522990 0.765911 0.094 Uiso 0.897(6) 1 calc R U P B 1 H3B H 0.208713 0.594415 0.773728 0.094 Uiso 0.897(6) 1 calc R U P B 1 H3C H 0.324135 0.561951 0.796252 0.094 Uiso 0.897(6) 1 calc R U P B 1 C4 C 0.2853(10) 0.4994(2) 0.6091(5) 0.170(5) Uani 0.897(6) 1 d . . P B 1 H4A H 0.284467 0.502801 0.549455 0.255 Uiso 0.897(6) 1 calc R U P B 1 H4B H 0.240816 0.464912 0.611650 0.255 Uiso 0.897(6) 1 calc R U P B 1 H4C H 0.360823 0.493805 0.651745 0.255 Uiso 0.897(6) 1 calc R U P B 1 Si1 Si 0.22789(17) 0.56917(13) 0.63652(8) 0.0528(6) Uani 0.897(6) 1 d . . P B 1 C3A C 0.212(4) 0.607(3) 0.759(2) 0.0623(15) Uani 0.103(6) 1 d . . P B 2 H3A1 H 0.290939 0.609112 0.796619 0.094 Uiso 0.103(6) 1 calc R U P B 2 H3A2 H 0.179965 0.572719 0.777442 0.094 Uiso 0.103(6) 1 calc R U P B 2 H3A3 H 0.176749 0.644143 0.766347 0.094 Uiso 0.103(6) 1 calc R U P B 2 C2A C 0.065(5) 0.624(5) 0.592(4) 0.170(5) Uani 0.103(6) 1 d . . P B 2 H2A1 H 0.053638 0.656635 0.627572 0.255 Uiso 0.103(6) 1 calc R U P B 2 H2A2 H 0.013368 0.591386 0.587216 0.255 Uiso 0.103(6) 1 calc R U P B 2 H2A3 H 0.053501 0.638871 0.533298 0.255 Uiso 0.103(6) 1 calc R U P B 2 Si1A Si 0.1929(11) 0.5982(7) 0.6416(6) 0.036(3) Uani 0.103(6) 1 d . . P B 2 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 C1 0.0445(18) 0.0421(18) 0.0197(13) -0.0039(12) 0.0055(12) -0.0070(14) C5 0.0223(13) 0.0194(13) 0.0250(13) 0.0029(10) 0.0014(11) -0.0024(10) C6 0.0246(13) 0.0174(12) 0.0219(12) 0.0026(9) 0.0043(11) 0.0008(10) C7 0.0242(13) 0.0191(12) 0.0211(12) 0.0029(10) 0.0048(10) 0.0023(10) C8 0.0244(13) 0.0193(13) 0.0216(13) 0.0013(10) 0.0043(11) -0.0002(10) C9 0.0276(14) 0.0176(12) 0.0207(12) 0.0013(10) 0.0023(11) -0.0004(10) C10 0.0279(14) 0.0214(13) 0.0227(13) 0.0045(10) 0.0072(11) 0.0026(11) C11 0.0235(13) 0.0223(13) 0.0270(13) 0.0027(10) 0.0061(11) -0.0015(10) C12 0.0231(14) 0.0294(14) 0.0239(13) -0.0034(11) 0.0051(11) -0.0039(11) C13 0.0330(16) 0.0372(16) 0.0295(15) -0.0008(12) 0.0098(12) -0.0116(12) C14 0.0224(14) 0.0427(17) 0.0374(16) -0.0056(13) 0.0078(12) -0.0020(12) C15 0.0276(15) 0.0381(16) 0.0288(14) -0.0042(12) 0.0054(12) -0.0094(12) C16 0.0363(16) 0.0322(15) 0.0256(14) -0.0032(11) 0.0136(12) -0.0051(12) C17 0.058(2) 0.0383(18) 0.0502(19) -0.0079(14) 0.0343(17) -0.0017(15) C18 0.059(2) 0.0448(19) 0.0248(14) 0.0008(13) 0.0154(14) -0.0023(16) C19 0.047(2) 0.064(2) 0.0397(18) -0.0049(16) 0.0258(16) -0.0081(16) C20 0.0250(14) 0.0321(15) 0.0224(13) -0.0027(11) 0.0036(11) -0.0062(11) C21 0.0317(16) 0.0452(18) 0.0297(15) 0.0022(13) -0.0022(13) -0.0024(14) C22 0.0362(18) 0.072(3) 0.0291(16) 0.0022(16) -0.0073(14) -0.0085(17) C23 0.043(2) 0.067(2) 0.0361(18) -0.0166(16) 0.0056(15) -0.0255(17) C24 0.0447(19) 0.0417(18) 0.0352(16) -0.0132(13) 0.0145(15) -0.0186(14) C25 0.0333(15) 0.0298(15) 0.0270(14) -0.0059(11) 0.0103(12) -0.0076(12) C26 0.044(2) 0.045(2) 0.0435(19) 0.0139(15) -0.0053(16) 0.0080(15) C27 0.066(3) 0.055(2) 0.045(2) 0.0097(17) -0.0074(19) 0.0172(19) C28 0.065(3) 0.058(2) 0.049(2) 0.0216(18) 0.0047(19) 0.0149(19) C29 0.0410(17) 0.0234(14) 0.0333(15) -0.0025(11) 0.0080(13) -0.0068(12) C30 0.069(2) 0.0306(17) 0.056(2) 0.0016(15) 0.0258(19) 0.0039(16) C31 0.058(2) 0.0401(18) 0.0324(16) 0.0004(13) 0.0130(15) -0.0047(15) C32 0.065(2) 0.049(2) 0.0450(19) -0.0014(15) 0.0285(18) 0.0112(18) C33 0.090(3) 0.053(2) 0.082(3) 0.001(2) 0.053(3) 0.027(2) C34 0.072(3) 0.057(3) 0.082(3) 0.019(2) 0.034(2) 0.031(2) C35 0.057(2) 0.047(2) 0.054(2) 0.0100(17) 0.0101(18) 0.0123(17) C36 0.0461(19) 0.0361(17) 0.0375(17) 0.0031(13) 0.0098(15) 0.0049(14) C37 0.152(6) 0.172(7) 0.096(5) -0.019(5) 0.056(5) -0.031(6) C38 0.149(7) 0.364(16) 0.097(6) -0.052(8) 0.066(6) -0.044(9) O2 0.210(7) 0.306(9) 0.120(5) 0.010(5) 0.079(5) -0.030(6) C40 0.092(4) 0.176(7) 0.087(4) -0.003(4) 0.021(4) -0.020(4) C41 0.133(6) 0.388(15) 0.070(4) -0.026(6) 0.043(4) -0.133(8) Fe1 0.0316(2) 0.0267(2) 0.0190(2) -0.00255(16) 0.00596(17) -0.00378(18) N1 0.0247(12) 0.0208(11) 0.0234(11) 0.0003(8) 0.0023(9) -0.0022(9) N2 0.0370(14) 0.0298(13) 0.0341(13) -0.0016(10) 0.0160(11) 0.0000(10) O1 0.0274(10) 0.0289(10) 0.0237(9) -0.0034(7) 0.0086(8) -0.0049(8) C2 0.092(5) 0.372(15) 0.035(3) -0.014(5) 0.014(3) -0.124(7) C3 0.053(3) 0.101(4) 0.034(2) 0.003(2) 0.0176(19) -0.025(3) C4 0.410(16) 0.035(3) 0.115(5) -0.002(3) 0.157(8) -0.013(5) Si1 0.0667(10) 0.0678(14) 0.0292(6) -0.0115(6) 0.0247(6) -0.0326(9) C3A 0.053(3) 0.101(4) 0.034(2) 0.003(2) 0.0176(19) -0.025(3) C2A 0.092(5) 0.372(15) 0.035(3) -0.014(5) 0.014(3) -0.124(7) Si1A 0.052(6) 0.034(6) 0.019(4) -0.014(4) 0.010(4) -0.003(5) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag C1 Si1A 1.764(12) . ? C1 Si1 1.815(3) . ? C1 Fe1 2.067(3) . ? C1 H1A 0.9700 . ? C1 H1B 0.9700 . ? C5 N1 1.292(3) . ? C5 C6 1.442(3) . ? C5 H5 0.9300 . ? C6 C11 1.413(4) . ? C6 C7 1.416(4) . ? C7 O1 1.315(3) . ? C7 C8 1.436(3) . ? C8 C9 1.387(4) . ? C8 C12 1.536(4) . ? C9 C10 1.414(4) . ? C9 H9 0.9300 . ? C10 C11 1.369(4) . ? C10 C16 1.535(4) . ? C11 H11 0.9300 . ? C12 C13 1.533(4) . ? C12 C15 1.535(4) . ? C12 C14 1.541(4) . ? C13 H13A 0.9600 . ? C13 H13B 0.9600 . ? C13 H13C 0.9600 . ? C14 H14A 0.9600 . ? C14 H14B 0.9600 . ? C14 H14C 0.9600 . ? C15 H15A 0.9600 . ? C15 H15B 0.9600 . ? C15 H15C 0.9600 . ? C16 C19 1.530(4) . ? C16 C18 1.535(4) . ? C16 C17 1.536(4) . ? C17 H17A 0.9600 . ? C17 H17B 0.9600 . ? C17 H17C 0.9600 . ? C18 H18A 0.9600 . ? C18 H18B 0.9600 . ? C18 H18C 0.9600 . ? C19 H19A 0.9600 . ? C19 H19B 0.9600 . ? C19 H19C 0.9600 . ? C20 C25 1.401(4) . ? C20 C21 1.405(4) . ? C20 N1 1.436(3) . ? C21 C22 1.393(4) . ? C21 C26 1.517(5) . ? C22 C23 1.389(5) . ? C22 H22 0.9300 . ? C23 C24 1.373(5) . ? C23 H23 0.9300 . ? C24 C25 1.394(4) . ? C24 H24 0.9300 . ? C25 C29 1.519(4) . ? C26 C27 1.514(6) . ? C26 C28 1.532(5) . ? C26 H26 0.9800 . ? C27 H27A 0.9600 . ? C27 H27B 0.9600 . ? C27 H27C 0.9600 . ? C28 H28A 0.9600 . ? C28 H28B 0.9600 . ? C28 H28C 0.9600 . ? C29 C31 1.527(4) . ? C29 C30 1.530(4) . ? C29 H29 0.9800 . ? C30 H30A 0.9600 . ? C30 H30B 0.9600 . ? C30 H30C 0.9600 . ? C31 H31A 0.9600 . ? C31 H31B 0.9600 . ? C31 H31C 0.9600 . ? C32 N2 1.342(4) . ? C32 C33 1.380(5) . ? C32 H32 0.9300 . ? C33 C34 1.362(6) . ? C33 H33 0.9300 . ? C34 C35 1.365(6) . ? C34 H34 0.9300 . ? C35 C36 1.378(5) . ? C35 H35 0.9300 . ? C36 N2 1.341(4) . ? C36 H36 0.9300 . ? C37 C38 1.455(9) . ? C37 H37A 0.9600 . ? C37 H37B 0.9600 . ? C37 H37C 0.9600 . ? C38 O2 1.358(8) . ? C38 H38A 0.9700 . ? C38 H38B 0.9700 . ? O2 C40 1.402(8) . ? C40 C41 1.389(8) . ? C40 H40A 0.9700 . ? C40 H40B 0.9700 . ? C41 H41A 0.9600 . ? C41 H41B 0.9600 . ? C41 H41C 0.9600 . ? Fe1 O1 1.9311(18) . ? Fe1 N1 2.052(2) . ? Fe1 N2 2.135(2) . ? C2 Si1 1.845(7) . ? C2 H2A 0.9600 . ? C2 H2B 0.9600 . ? C2 H2C 0.9600 . ? C3 Si1 1.887(4) . ? C3 H3A 0.9600 . ? C3 H3B 0.9600 . ? C3 H3C 0.9600 . ? C4 Si1 1.825(7) . ? C4 H4A 0.9600 . ? C4 H4B 0.9600 . ? C4 H4C 0.9600 . ? C3A Si1A 1.83(4) . ? C3A H3A1 0.9600 . ? C3A H3A2 0.9600 . ? C3A H3A3 0.9600 . ? C2A Si1A 1.63(8) . ? C2A H2A1 0.9600 . ? C2A H2A2 0.9600 . ? C2A H2A3 0.9600 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag Si1A C1 Fe1 118.4(3) . . ? Si1 C1 Fe1 113.22(15) . . ? Si1 C1 H1A 108.9 . . ? Fe1 C1 H1A 108.9 . . ? Si1 C1 H1B 108.9 . . ? Fe1 C1 H1B 108.9 . . ? H1A C1 H1B 107.7 . . ? N1 C5 C6 127.8(2) . . ? N1 C5 H5 116.1 . . ? C6 C5 H5 116.1 . . ? C11 C6 C7 120.7(2) . . ? C11 C6 C5 116.2(2) . . ? C7 C6 C5 123.1(2) . . ? O1 C7 C6 121.7(2) . . ? O1 C7 C8 120.3(2) . . ? C6 C7 C8 118.0(2) . . ? C9 C8 C7 118.0(2) . . ? C9 C8 C12 121.5(2) . . ? C7 C8 C12 120.5(2) . . ? C8 C9 C10 124.6(2) . . ? C8 C9 H9 117.7 . . ? C10 C9 H9 117.7 . . ? C11 C10 C9 116.5(2) . . ? C11 C10 C16 123.3(2) . . ? C9 C10 C16 120.2(2) . . ? C10 C11 C6 122.1(2) . . ? C10 C11 H11 118.9 . . ? C6 C11 H11 118.9 . . ? C13 C12 C15 106.9(2) . . ? C13 C12 C8 109.9(2) . . ? C15 C12 C8 112.1(2) . . ? C13 C12 C14 110.0(2) . . ? C15 C12 C14 107.0(2) . . ? C8 C12 C14 110.8(2) . . ? C12 C13 H13A 109.5 . . ? C12 C13 H13B 109.5 . . ? H13A C13 H13B 109.5 . . ? C12 C13 H13C 109.5 . . ? H13A C13 H13C 109.5 . . ? H13B C13 H13C 109.5 . . ? C12 C14 H14A 109.5 . . ? C12 C14 H14B 109.5 . . ? H14A C14 H14B 109.5 . . ? C12 C14 H14C 109.5 . . ? H14A C14 H14C 109.5 . . ? H14B C14 H14C 109.5 . . ? C12 C15 H15A 109.5 . . ? C12 C15 H15B 109.5 . . ? H15A C15 H15B 109.5 . . ? C12 C15 H15C 109.5 . . ? H15A C15 H15C 109.5 . . ? H15B C15 H15C 109.5 . . ? C19 C16 C18 108.4(3) . . ? C19 C16 C10 111.6(2) . . ? C18 C16 C10 108.5(2) . . ? C19 C16 C17 108.7(3) . . ? C18 C16 C17 109.3(2) . . ? C10 C16 C17 110.2(2) . . ? C16 C17 H17A 109.5 . . ? C16 C17 H17B 109.5 . . ? H17A C17 H17B 109.5 . . ? C16 C17 H17C 109.5 . . ? H17A C17 H17C 109.5 . . ? H17B C17 H17C 109.5 . . ? C16 C18 H18A 109.5 . . ? C16 C18 H18B 109.5 . . ? H18A C18 H18B 109.5 . . ? C16 C18 H18C 109.5 . . ? H18A C18 H18C 109.5 . . ? H18B C18 H18C 109.5 . . ? C16 C19 H19A 109.5 . . ? C16 C19 H19B 109.5 . . ? H19A C19 H19B 109.5 . . ? C16 C19 H19C 109.5 . . ? H19A C19 H19C 109.5 . . ? H19B C19 H19C 109.5 . . ? C25 C20 C21 122.3(3) . . ? C25 C20 N1 119.1(2) . . ? C21 C20 N1 118.5(2) . . ? C22 C21 C20 117.1(3) . . ? C22 C21 C26 122.2(3) . . ? C20 C21 C26 120.7(3) . . ? C23 C22 C21 121.4(3) . . ? C23 C22 H22 119.3 . . ? C21 C22 H22 119.3 . . ? C24 C23 C22 120.3(3) . . ? C24 C23 H23 119.9 . . ? C22 C23 H23 119.9 . . ? C23 C24 C25 120.9(3) . . ? C23 C24 H24 119.6 . . ? C25 C24 H24 119.6 . . ? C24 C25 C20 118.0(3) . . ? C24 C25 C29 120.2(3) . . ? C20 C25 C29 121.8(2) . . ? C27 C26 C21 111.5(3) . . ? C27 C26 C28 109.6(3) . . ? C21 C26 C28 113.4(3) . . ? C27 C26 H26 107.3 . . ? C21 C26 H26 107.3 . . ? C28 C26 H26 107.3 . . ? C26 C27 H27A 109.5 . . ? C26 C27 H27B 109.5 . . ? H27A C27 H27B 109.5 . . ? C26 C27 H27C 109.5 . . ? H27A C27 H27C 109.5 . . ? H27B C27 H27C 109.5 . . ? C26 C28 H28A 109.5 . . ? C26 C28 H28B 109.5 . . ? H28A C28 H28B 109.5 . . ? C26 C28 H28C 109.5 . . ? H28A C28 H28C 109.5 . . ? H28B C28 H28C 109.5 . . ? C25 C29 C31 110.7(3) . . ? C25 C29 C30 112.6(3) . . ? C31 C29 C30 110.6(3) . . ? C25 C29 H29 107.6 . . ? C31 C29 H29 107.6 . . ? C30 C29 H29 107.6 . . ? C29 C30 H30A 109.5 . . ? C29 C30 H30B 109.5 . . ? H30A C30 H30B 109.5 . . ? C29 C30 H30C 109.5 . . ? H30A C30 H30C 109.5 . . ? H30B C30 H30C 109.5 . . ? C29 C31 H31A 109.5 . . ? C29 C31 H31B 109.5 . . ? H31A C31 H31B 109.5 . . ? C29 C31 H31C 109.5 . . ? H31A C31 H31C 109.5 . . ? H31B C31 H31C 109.5 . . ? N2 C32 C33 122.6(3) . . ? N2 C32 H32 118.7 . . ? C33 C32 H32 118.7 . . ? C34 C33 C32 119.7(4) . . ? C34 C33 H33 120.1 . . ? C32 C33 H33 120.1 . . ? C33 C34 C35 118.7(4) . . ? C33 C34 H34 120.6 . . ? C35 C34 H34 120.6 . . ? C34 C35 C36 119.0(4) . . ? C34 C35 H35 120.5 . . ? C36 C35 H35 120.5 . . ? N2 C36 C35 123.4(3) . . ? N2 C36 H36 118.3 . . ? C35 C36 H36 118.3 . . ? C38 C37 H37A 109.5 . . ? C38 C37 H37B 109.5 . . ? H37A C37 H37B 109.5 . . ? C38 C37 H37C 109.5 . . ? H37A C37 H37C 109.5 . . ? H37B C37 H37C 109.5 . . ? O2 C38 C37 129.6(8) . . ? O2 C38 H38A 104.9 . . ? C37 C38 H38A 104.9 . . ? O2 C38 H38B 104.9 . . ? C37 C38 H38B 104.9 . . ? H38A C38 H38B 105.8 . . ? C38 O2 C40 132.8(7) . . ? O2 C40 C41 129.0(6) . . ? O2 C40 H40A 105.0 . . ? C41 C40 H40A 105.0 . . ? O2 C40 H40B 105.0 . . ? C41 C40 H40B 105.0 . . ? H40A C40 H40B 105.9 . . ? C40 C41 H41A 109.5 . . ? C40 C41 H41B 109.5 . . ? H41A C41 H41B 109.5 . . ? C40 C41 H41C 109.5 . . ? H41A C41 H41C 109.5 . . ? H41B C41 H41C 109.5 . . ? O1 Fe1 N1 89.35(8) . . ? O1 Fe1 C1 136.48(10) . . ? N1 Fe1 C1 116.32(11) . . ? O1 Fe1 N2 96.77(8) . . ? N1 Fe1 N2 107.11(9) . . ? C1 Fe1 N2 107.06(11) . . ? C5 N1 C20 116.8(2) . . ? C5 N1 Fe1 124.57(18) . . ? C20 N1 Fe1 118.66(17) . . ? C36 N2 C32 116.7(3) . . ? C36 N2 Fe1 120.2(2) . . ? C32 N2 Fe1 123.0(2) . . ? C7 O1 Fe1 132.88(16) . . ? Si1 C2 H2A 109.5 . . ? Si1 C2 H2B 109.5 . . ? H2A C2 H2B 109.5 . . ? Si1 C2 H2C 109.5 . . ? H2A C2 H2C 109.5 . . ? H2B C2 H2C 109.5 . . ? Si1 C3 H3A 109.5 . . ? Si1 C3 H3B 109.5 . . ? H3A C3 H3B 109.5 . . ? Si1 C3 H3C 109.5 . . ? H3A C3 H3C 109.5 . . ? H3B C3 H3C 109.5 . . ? Si1 C4 H4A 109.5 . . ? Si1 C4 H4B 109.5 . . ? H4A C4 H4B 109.5 . . ? Si1 C4 H4C 109.5 . . ? H4A C4 H4C 109.5 . . ? H4B C4 H4C 109.5 . . ? C1 Si1 C4 110.8(3) . . ? C1 Si1 C2 109.5(3) . . ? C4 Si1 C2 106.6(5) . . ? C1 Si1 C3 113.21(18) . . ? C4 Si1 C3 106.1(3) . . ? C2 Si1 C3 110.4(2) . . ? Si1A C3A H3A1 109.5 . . ? Si1A C3A H3A2 109.5 . . ? H3A1 C3A H3A2 109.5 . . ? Si1A C3A H3A3 109.5 . . ? H3A1 C3A H3A3 109.5 . . ? H3A2 C3A H3A3 109.5 . . ? Si1A C2A H2A1 109.5 . . ? Si1A C2A H2A2 109.5 . . ? H2A1 C2A H2A2 109.5 . . ? Si1A C2A H2A3 109.5 . . ? H2A1 C2A H2A3 109.5 . . ? H2A2 C2A H2A3 109.5 . . ? C2A Si1A C1 117(3) . . ? C2A Si1A C3A 100(3) . . ? C1 Si1A C3A 112.7(14) . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag N1 C5 C6 C11 176.6(2) . . . . ? N1 C5 C6 C7 -3.4(4) . . . . ? C11 C6 C7 O1 178.0(2) . . . . ? C5 C6 C7 O1 -2.0(4) . . . . ? C11 C6 C7 C8 -2.4(3) . . . . ? C5 C6 C7 C8 177.5(2) . . . . ? O1 C7 C8 C9 -179.5(2) . . . . ? C6 C7 C8 C9 0.9(3) . . . . ? O1 C7 C8 C12 -0.3(4) . . . . ? C6 C7 C8 C12 -179.9(2) . . . . ? C7 C8 C9 C10 0.9(4) . . . . ? C12 C8 C9 C10 -178.3(2) . . . . ? C8 C9 C10 C11 -1.1(4) . . . . ? C8 C9 C10 C16 -179.7(2) . . . . ? C9 C10 C11 C6 -0.4(4) . . . . ? C16 C10 C11 C6 178.1(2) . . . . ? C7 C6 C11 C10 2.2(4) . . . . ? C5 C6 C11 C10 -177.7(2) . . . . ? C9 C8 C12 C13 116.8(3) . . . . ? C7 C8 C12 C13 -62.4(3) . . . . ? C9 C8 C12 C15 -1.9(3) . . . . ? C7 C8 C12 C15 178.9(2) . . . . ? C9 C8 C12 C14 -121.5(3) . . . . ? C7 C8 C12 C14 59.4(3) . . . . ? C11 C10 C16 C19 9.2(4) . . . . ? C9 C10 C16 C19 -172.3(3) . . . . ? C11 C10 C16 C18 -110.3(3) . . . . ? C9 C10 C16 C18 68.2(3) . . . . ? C11 C10 C16 C17 130.1(3) . . . . ? C9 C10 C16 C17 -51.4(3) . . . . ? C25 C20 C21 C22 -1.6(5) . . . . ? N1 C20 C21 C22 -179.3(3) . . . . ? C25 C20 C21 C26 -179.5(3) . . . . ? N1 C20 C21 C26 2.9(5) . . . . ? C20 C21 C22 C23 0.3(5) . . . . ? C26 C21 C22 C23 178.1(4) . . . . ? C21 C22 C23 C24 1.0(6) . . . . ? C22 C23 C24 C25 -0.9(5) . . . . ? C23 C24 C25 C20 -0.4(5) . . . . ? C23 C24 C25 C29 -178.4(3) . . . . ? C21 C20 C25 C24 1.7(4) . . . . ? N1 C20 C25 C24 179.3(3) . . . . ? C21 C20 C25 C29 179.7(3) . . . . ? N1 C20 C25 C29 -2.7(4) . . . . ? C22 C21 C26 C27 -92.2(4) . . . . ? C20 C21 C26 C27 85.6(4) . . . . ? C22 C21 C26 C28 32.1(5) . . . . ? C20 C21 C26 C28 -150.1(3) . . . . ? C24 C25 C29 C31 73.2(3) . . . . ? C20 C25 C29 C31 -104.8(3) . . . . ? C24 C25 C29 C30 -51.2(4) . . . . ? C20 C25 C29 C30 130.9(3) . . . . ? N2 C32 C33 C34 1.3(7) . . . . ? C32 C33 C34 C35 -1.4(7) . . . . ? C33 C34 C35 C36 0.5(7) . . . . ? C34 C35 C36 N2 0.5(6) . . . . ? C37 C38 O2 C40 -175.2(10) . . . . ? C38 O2 C40 C41 179.2(12) . . . . ? C6 C5 N1 C20 -179.0(2) . . . . ? C6 C5 N1 Fe1 2.1(4) . . . . ? C25 C20 N1 C5 86.6(3) . . . . ? C21 C20 N1 C5 -95.7(3) . . . . ? C25 C20 N1 Fe1 -94.4(3) . . . . ? C21 C20 N1 Fe1 83.3(3) . . . . ? C35 C36 N2 C32 -0.7(5) . . . . ? C35 C36 N2 Fe1 175.0(3) . . . . ? C33 C32 N2 C36 -0.2(5) . . . . ? C33 C32 N2 Fe1 -175.8(3) . . . . ? C6 C7 O1 Fe1 9.0(4) . . . . ? C8 C7 O1 Fe1 -170.57(17) . . . . ? Fe1 C1 Si1 C4 63.3(4) . . . . ? Fe1 C1 Si1 C2 -54.0(4) . . . . ? Fe1 C1 Si1 C3 -177.6(2) . . . . ? Fe1 C1 Si1A C2A -53(3) . . . . ? Fe1 C1 Si1A C3A -167.5(19) . . . . ? _refine_diff_density_max 0.634 _refine_diff_density_min -0.460 _refine_diff_density_rms 0.057 _shelx_res_file ; TITL POP5_a.res in P2(1)/n shelx.res created by SHELXL-2018/3 at 16:22:53 on 21-Nov-2021 CELL 1.54178 13.0003 21.8240 16.1198 90.000 113.115 90.000 ZERR 4.00 0.0002 0.0004 0.0003 0.000 0.001 0.000 LATT 1 SYMM 1/2 - X, 1/2 + Y, 1/2 - Z SFAC C H FE N O SI UNIT 163.596 262.79 4 8 4 4 MERG 2 EADP C2 C2A EADP C3 C3A FMAP 2 PLAN 20 SIZE 0.122 0.209 0.241 ACTA BOND $H CONF LIST 6 L.S. 32 TEMP 0.00 WGHT 0.069900 3.746800 FVAR 0.36155 0.89740 C1 1 0.296515 0.636483 0.616051 11.00000 0.04454 0.04208 = 0.01966 -0.00388 0.00554 -0.00698 AFIX 23 H1A 2 0.376179 0.633569 0.651939 11.00000 -1.20000 H1B 2 0.268780 0.672543 0.635806 11.00000 -1.20000 AFIX 0 C5 1 0.425951 0.645022 0.385947 11.00000 0.02235 0.01943 = 0.02495 0.00286 0.00141 -0.00239 AFIX 43 H5 2 0.494178 0.654812 0.383222 11.00000 -1.20000 AFIX 0 C6 1 0.349456 0.610144 0.311224 11.00000 0.02463 0.01738 = 0.02191 0.00256 0.00429 0.00083 C7 1 0.244766 0.588842 0.307299 11.00000 0.02418 0.01910 = 0.02108 0.00287 0.00476 0.00226 C8 1 0.173760 0.556658 0.227724 11.00000 0.02435 0.01925 = 0.02164 0.00127 0.00433 -0.00023 C9 1 0.212640 0.547532 0.159906 11.00000 0.02762 0.01762 = 0.02073 0.00129 0.00231 -0.00036 AFIX 43 H9 2 0.165983 0.527155 0.108123 11.00000 -1.20000 AFIX 0 C10 1 0.318217 0.567035 0.163990 11.00000 0.02792 0.02136 = 0.02275 0.00448 0.00719 0.00263 C11 1 0.384432 0.597862 0.240244 11.00000 0.02350 0.02233 = 0.02696 0.00272 0.00608 -0.00146 AFIX 43 H11 2 0.454696 0.611149 0.245498 11.00000 -1.20000 AFIX 0 C12 1 0.059110 0.532539 0.219395 11.00000 0.02311 0.02941 = 0.02387 -0.00339 0.00515 -0.00386 C13 1 0.074227 0.484909 0.293213 11.00000 0.03297 0.03719 = 0.02949 -0.00085 0.00982 -0.01165 AFIX 137 H13A 2 0.116611 0.450859 0.285819 11.00000 -1.50000 H13B 2 0.002235 0.470863 0.288686 11.00000 -1.50000 H13C 2 0.113298 0.503188 0.351348 11.00000 -1.50000 AFIX 0 C14 1 -0.015630 0.585357 0.226532 11.00000 0.02238 0.04272 = 0.03736 -0.00564 0.00784 -0.00200 AFIX 137 H14A 2 0.016330 0.602872 0.285869 11.00000 -1.50000 H14B 2 -0.088967 0.569908 0.215570 11.00000 -1.50000 H14C 2 -0.020823 0.616202 0.182603 11.00000 -1.50000 AFIX 0 C15 1 -0.004026 0.500703 0.128546 11.00000 0.02759 0.03812 = 0.02877 -0.00424 0.00541 -0.00940 AFIX 137 H15A 2 -0.015365 0.529194 0.080368 11.00000 -1.50000 H15B 2 -0.075159 0.486525 0.125886 11.00000 -1.50000 H15C 2 0.038968 0.466484 0.122578 11.00000 -1.50000 AFIX 0 C16 1 0.352465 0.554687 0.084574 11.00000 0.03627 0.03219 = 0.02558 -0.00321 0.01364 -0.00506 C17 1 0.335821 0.486670 0.058128 11.00000 0.05832 0.03829 = 0.05019 -0.00795 0.03433 -0.00166 AFIX 137 H17A 2 0.382791 0.462099 0.108018 11.00000 -1.50000 H17B 2 0.355278 0.479752 0.007273 11.00000 -1.50000 H17C 2 0.258994 0.475651 0.042566 11.00000 -1.50000 AFIX 0 C18 1 0.278771 0.593841 0.004107 11.00000 0.05857 0.04485 = 0.02482 0.00075 0.01543 -0.00231 AFIX 137 H18A 2 0.201623 0.583449 -0.011701 11.00000 -1.50000 H18B 2 0.298549 0.586150 -0.046403 11.00000 -1.50000 H18C 2 0.290036 0.636419 0.020085 11.00000 -1.50000 AFIX 0 C19 1 0.474843 0.571563 0.107697 11.00000 0.04676 0.06378 = 0.03967 -0.00487 0.02578 -0.00815 AFIX 137 H19A 2 0.485570 0.614453 0.121659 11.00000 -1.50000 H19B 2 0.493748 0.562716 0.057056 11.00000 -1.50000 H19C 2 0.522010 0.548111 0.158888 11.00000 -1.50000 AFIX 0 C20 1 0.500540 0.699230 0.520654 11.00000 0.02503 0.03215 = 0.02240 -0.00268 0.00357 -0.00623 C21 1 0.578737 0.668661 0.595600 11.00000 0.03175 0.04522 = 0.02974 0.00219 -0.00216 -0.00239 C22 1 0.663679 0.703937 0.657400 11.00000 0.03624 0.07226 = 0.02912 0.00221 -0.00727 -0.00850 AFIX 43 H22 2 0.717049 0.685117 0.707647 11.00000 -1.20000 AFIX 0 C23 1 0.670309 0.766635 0.645527 11.00000 0.04319 0.06651 = 0.03606 -0.01660 0.00562 -0.02555 AFIX 43 H23 2 0.728405 0.789155 0.687201 11.00000 -1.20000 AFIX 0 C24 1 0.591448 0.795519 0.572515 11.00000 0.04472 0.04175 = 0.03518 -0.01316 0.01446 -0.01861 AFIX 43 H24 2 0.596110 0.837613 0.565701 11.00000 -1.20000 AFIX 0 C25 1 0.504541 0.762602 0.508506 11.00000 0.03334 0.02983 = 0.02697 -0.00589 0.01027 -0.00762 C26 1 0.572035 0.599835 0.605842 11.00000 0.04393 0.04462 = 0.04353 0.01387 -0.00531 0.00799 AFIX 13 H26 2 0.492860 0.588377 0.578207 11.00000 -1.20000 AFIX 0 C27 1 0.631590 0.565730 0.555906 11.00000 0.06608 0.05472 = 0.04517 0.00967 -0.00740 0.01724 AFIX 137 H27A 2 0.596115 0.574607 0.492618 11.00000 -1.50000 H27B 2 0.628045 0.522478 0.565305 11.00000 -1.50000 H27C 2 0.708384 0.578475 0.578121 11.00000 -1.50000 AFIX 0 C28 1 0.616844 0.578573 0.704258 11.00000 0.06512 0.05799 = 0.04859 0.02161 0.00467 0.01489 AFIX 137 H28A 2 0.696280 0.584795 0.731430 11.00000 -1.50000 H28B 2 0.600604 0.535840 0.706491 11.00000 -1.50000 H28C 2 0.581734 0.601757 0.736539 11.00000 -1.50000 AFIX 0 C29 1 0.419760 0.795024 0.426910 11.00000 0.04104 0.02340 = 0.03327 -0.00247 0.00802 -0.00683 AFIX 13 H29 2 0.358641 0.766196 0.396716 11.00000 -1.20000 AFIX 0 C30 1 0.369276 0.851599 0.452586 11.00000 0.06924 0.03061 = 0.05624 0.00158 0.02580 0.00391 AFIX 137 H30A 2 0.336790 0.840098 0.494489 11.00000 -1.50000 H30B 2 0.312511 0.868696 0.399427 11.00000 -1.50000 H30C 2 0.426843 0.881510 0.479956 11.00000 -1.50000 AFIX 0 C31 1 0.471761 0.812003 0.359937 11.00000 0.05843 0.04013 = 0.03242 0.00038 0.01297 -0.00468 AFIX 137 H31A 2 0.534274 0.838815 0.388621 11.00000 -1.50000 H31B 2 0.417007 0.832367 0.308880 11.00000 -1.50000 H31C 2 0.496686 0.775500 0.340215 11.00000 -1.50000 AFIX 0 C32 1 0.138751 0.763372 0.485584 11.00000 0.06517 0.04933 = 0.04500 -0.00143 0.02848 0.01122 AFIX 43 H32 2 0.175876 0.759240 0.547725 11.00000 -1.20000 AFIX 0 C33 1 0.062288 0.810286 0.452303 11.00000 0.09010 0.05290 = 0.08193 0.00085 0.05299 0.02685 AFIX 43 H33 2 0.049705 0.837558 0.491656 11.00000 -1.20000 AFIX 0 C34 1 0.005371 0.816452 0.361601 11.00000 0.07164 0.05711 = 0.08223 0.01897 0.03374 0.03095 AFIX 43 H34 2 -0.047559 0.847299 0.338286 11.00000 -1.20000 AFIX 0 C35 1 0.027463 0.776515 0.305558 11.00000 0.05682 0.04684 = 0.05423 0.00998 0.01007 0.01232 AFIX 43 H35 2 -0.009750 0.779905 0.243323 11.00000 -1.20000 AFIX 0 C36 1 0.105802 0.731066 0.342630 11.00000 0.04609 0.03608 = 0.03751 0.00311 0.00984 0.00491 AFIX 43 H36 2 0.120723 0.704287 0.303862 11.00000 -1.20000 AFIX 0 C37 1 0.902785 0.716685 0.580144 11.00000 0.15178 0.17154 = 0.09633 -0.01908 0.05569 -0.03055 AFIX 137 H37A 2 0.966549 0.691627 0.587729 11.00000 -1.50000 H37B 2 0.879614 0.709322 0.628950 11.00000 -1.50000 H37C 2 0.922292 0.759090 0.579886 11.00000 -1.50000 AFIX 0 C38 1 0.811668 0.701550 0.495042 11.00000 0.14888 0.36413 = 0.09691 -0.05194 0.06590 -0.04409 AFIX 23 H38A 2 0.788581 0.660609 0.503713 11.00000 -1.20000 H38B 2 0.750841 0.728426 0.491952 11.00000 -1.20000 AFIX 0 O2 5 0.809499 0.701315 0.410113 11.00000 0.20976 0.30566 = 0.11958 0.01042 0.07931 -0.02975 C40 1 0.723979 0.691196 0.325165 11.00000 0.09155 0.17559 = 0.08710 -0.00317 0.02091 -0.02023 AFIX 23 H40A 2 0.665755 0.720214 0.321304 11.00000 -1.20000 H40B 2 0.694350 0.651038 0.329279 11.00000 -1.20000 AFIX 0 C41 1 0.729103 0.692564 0.240739 11.00000 0.13306 0.38763 = 0.06959 -0.02586 0.04336 -0.13328 AFIX 137 H41A 2 0.805387 0.687979 0.247381 11.00000 -1.50000 H41B 2 0.700411 0.730985 0.211959 11.00000 -1.50000 H41C 2 0.685054 0.659672 0.204516 11.00000 -1.50000 AFIX 0 FE1 3 0.271373 0.647214 0.482067 11.00000 0.03161 0.02671 = 0.01897 -0.00255 0.00596 -0.00378 N1 4 0.411158 0.664316 0.456233 11.00000 0.02466 0.02081 = 0.02336 0.00027 0.00234 -0.00223 N2 4 0.161603 0.723486 0.431737 11.00000 0.03704 0.02978 = 0.03414 -0.00158 0.01602 0.00001 O1 5 0.212008 0.598221 0.373761 11.00000 0.02738 0.02891 = 0.02366 -0.00344 0.00864 -0.00493 PART 1 C2 1 0.078090 0.570811 0.561733 21.00000 0.09164 0.37226 = 0.03541 -0.01407 0.01373 -0.12365 AFIX 137 H2A 2 0.070259 0.574604 0.500206 21.00000 -1.50000 H2B 2 0.042938 0.605123 0.577230 21.00000 -1.50000 H2C 2 0.043126 0.533561 0.568850 21.00000 -1.50000 AFIX 0 C3 1 0.245939 0.561146 0.758027 21.00000 0.05277 0.10128 = 0.03355 0.00254 0.01758 -0.02513 AFIX 137 H3A 2 0.214148 0.522990 0.765911 21.00000 -1.50000 H3B 2 0.208713 0.594415 0.773728 21.00000 -1.50000 H3C 2 0.324135 0.561951 0.796252 21.00000 -1.50000 AFIX 0 C4 1 0.285301 0.499407 0.609092 21.00000 0.41028 0.03540 = 0.11495 -0.00171 0.15693 -0.01313 AFIX 137 H4A 2 0.284467 0.502801 0.549455 21.00000 -1.50000 H4B 2 0.240816 0.464912 0.611650 21.00000 -1.50000 H4C 2 0.360823 0.493805 0.651745 21.00000 -1.50000 AFIX 0 SI1 6 0.227893 0.569169 0.636515 21.00000 0.06672 0.06779 = 0.02920 -0.01147 0.02467 -0.03261 PART 2 C3A 1 0.212464 0.607105 0.759477 -21.00000 0.05277 0.10128 = 0.03355 0.00254 0.01758 -0.02513 AFIX 137 H3A1 2 0.290939 0.609112 0.796619 -21.00000 -1.50000 H3A2 2 0.179965 0.572719 0.777442 -21.00000 -1.50000 H3A3 2 0.176749 0.644143 0.766347 -21.00000 -1.50000 AFIX 0 C2A 1 0.065199 0.623930 0.592340 -21.00000 0.09164 0.37226 = 0.03541 -0.01407 0.01373 -0.12365 AFIX 137 H2A1 2 0.053638 0.656635 0.627572 -21.00000 -1.50000 H2A2 2 0.013368 0.591386 0.587216 -21.00000 -1.50000 H2A3 2 0.053501 0.638871 0.533298 -21.00000 -1.50000 AFIX 0 SI1A 6 0.192944 0.598240 0.641559 -21.00000 0.05228 0.03391 = 0.01929 -0.01403 0.01014 -0.00291 HKLF 4 REM POP5_a.res in P2(1)/n REM wR2 = 0.1437, GooF = S = 1.037, Restrained GooF = 1.037 for all data REM R1 = 0.0523 for 5819 Fo > 4sig(Fo) and 0.0722 for all 7459 data REM 448 parameters refined using 0 restraints END WGHT 0.0712 3.9832 REM Highest difference peak 0.634, deepest hole -0.460, 1-sigma level 0.057 Q1 1 0.6723 0.7497 0.2823 11.00000 0.05 0.63 Q2 1 0.8029 0.6534 0.3353 11.00000 0.05 0.55 Q3 1 0.7373 0.6608 0.2573 11.00000 0.05 0.49 Q4 1 0.3417 0.6533 0.4606 11.00000 0.05 0.48 Q5 1 0.7136 0.7405 0.3750 11.00000 0.05 0.46 Q6 1 0.1856 0.5211 0.5976 11.00000 0.05 0.38 Q7 1 0.6610 0.7107 0.2041 11.00000 0.05 0.31 Q8 1 0.9013 0.7007 0.3986 11.00000 0.05 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4.50 4.70 5 -9 0 0.40 7.40 -5 -9 0 12.80 5.20 5 -9 0 6.00 4.90 5 -9 0 11.60 6.90 -5 -9 0 15.10 3.90 -5 -9 0 6.00 6.00 -5 -9 0 8.70 6.00 -5 -9 0 7.20 5.30 -5 -9 0 4.70 7.70 5 9 0 2.50 4.70 5 9 0 3.20 8.70 6 -9 0 224.28 13.20 6 -9 0 218.68 13.40 -6 -9 0 233.68 19.00 -6 -9 0 240.28 18.90 6 -9 0 181.08 19.00 6 -9 0 217.98 13.70 -6 -9 0 223.08 15.10 6 -9 0 234.18 13.50 -6 -9 0 215.88 14.70 6 -9 0 221.68 17.60 -6 -9 0 217.38 13.30 -6 -9 0 224.48 12.00 -6 -9 0 240.78 13.60 6 9 0 224.68 13.50 6 9 0 238.88 14.70 6 9 0 241.68 21.00 -7 -9 0 22.80 11.80 7 -9 0 41.30 10.20 7 -9 0 33.20 7.20 -7 -9 0 38.90 8.40 -7 -9 0 29.00 9.40 -7 -9 0 49.10 9.10 -7 -9 0 35.60 6.80 7 -9 0 48.40 9.30 7 -9 0 27.90 6.10 7 -9 0 32.30 13.10 -7 -9 0 41.00 7.40 7 -9 0 31.40 10.40 7 -9 0 34.50 7.40 -7 -9 0 37.00 7.70 7 9 0 49.10 12.60 -7 9 0 32.80 7.30 7 9 0 26.80 12.40 7 9 0 27.50 7.10 -8 -9 0 585.14 27.90 -8 -9 0 575.94 24.30 -8 -9 0 588.24 34.40 8 -9 0 558.24 28.70 -8 -9 0 598.34 28.10 8 -9 0 637.94 36.90 8 -9 0 602.34 26.30 8 -9 0 612.64 26.70 8 -9 0 598.14 32.60 -8 -9 0 574.64 25.60 8 9 0 568.74 37.90 -8 9 0 591.04 44.10 8 9 0 551.94 27.30 -8 9 0 589.44 25.90 9 -9 0 32.80 9.50 9 -9 0 33.00 8.10 9 -9 0 38.40 12.30 9 -9 0 39.60 9.70 -9 -9 0 43.00 9.50 -9 -9 0 67.19 9.60 9 -9 0 36.10 17.60 -9 -9 0 44.70 10.30 -9 -9 0 32.60 15.80 9 -9 0 54.79 10.40 9 9 0 43.80 10.30 9 9 0 39.40 16.20 -9 9 0 44.10 9.70 9 9 0 41.10 7.80 9 9 0 36.60 11.70 10 -9 0 98.79 24.10 -10 -9 0 86.89 16.80 -10 -9 0 108.69 26.20 10 -9 0 69.89 16.20 10 -9 0 59.39 11.80 -10 -9 0 70.89 18.50 10 -9 0 40.20 11.40 -10 9 0 120.19 21.40 -10 9 0 75.69 13.30 10 9 0 39.80 24.00 10 9 0 81.99 17.00 10 9 0 47.80 10.40 -11 -9 0 40.80 10.40 11 -9 0 91.69 20.00 11 -9 0 12.00 10.50 11 -9 0 47.00 11.10 11 -9 0 31.40 8.20 -11 -9 0 69.49 15.10 -11 9 0 44.00 12.30 -11 9 0 26.50 10.70 11 9 0 19.70 11.10 -11 9 0 44.40 11.20 12 -9 0 209.28 15.50 -12 -9 0 190.88 15.50 12 -9 0 157.18 15.10 12 -9 0 196.98 16.90 12 -9 0 246.28 22.00 -12 -9 0 203.68 16.90 -12 9 0 193.48 18.40 -12 9 0 161.08 16.50 12 9 0 198.88 13.60 -12 9 0 198.98 19.10 12 9 0 206.88 17.90 13 -9 0 76.09 15.30 -13 -9 0 23.60 7.10 13 -9 0 35.60 7.20 -13 -9 0 38.20 7.60 13 -9 0 27.50 7.50 13 9 0 26.40 7.30 -13 9 0 32.00 8.50 0 -10 0 19.00 5.00 0 -10 0 13.80 4.90 0 -10 0 29.00 4.70 0 10 0 18.30 5.40 -1 -10 0 12.60 5.80 -1 -10 0 10.50 4.20 1 -10 0 13.00 4.60 1 -10 0 13.60 4.10 1 -10 0 6.50 4.40 -1 -10 0 4.40 4.50 -1 10 0 6.60 6.70 -2 -10 0 869.61 35.60 2 -10 0 824.52 33.10 2 -10 0 876.41 35.70 2 -10 0 890.81 33.30 -2 -10 0 856.91 36.40 2 -10 0 877.21 35.00 2 10 0 911.61 37.20 -3 -10 0 167.98 13.00 3 -10 0 152.58 10.50 3 -10 0 156.88 13.70 -3 -10 0 186.28 12.10 -3 -10 0 154.28 13.60 3 10 0 143.99 10.90 3 10 0 173.38 16.60 -4 -10 0 21.00 5.60 -4 -10 0 18.10 5.70 -4 -10 0 25.60 8.00 4 -10 0 25.50 8.00 -4 -10 0 21.70 4.10 4 -10 0 23.40 4.40 4 -10 0 22.80 4.50 -4 -10 0 21.60 4.90 4 -10 0 39.70 8.20 -4 -10 0 12.30 6.00 4 10 0 21.80 4.80 4 10 0 20.90 9.10 5 -10 0 23.60 9.70 5 -10 0 40.70 8.80 -5 -10 0 39.00 6.00 -5 -10 0 37.30 9.90 5 -10 0 50.39 8.50 -5 -10 0 37.90 6.80 -5 -10 0 30.50 6.70 5 -10 0 32.00 5.70 5 -10 0 43.10 8.20 -5 -10 0 38.70 6.90 -5 -10 0 33.20 7.60 5 -10 0 45.80 8.10 -5 -10 0 51.09 8.60 5 10 0 24.10 5.80 5 10 0 43.30 11.10 -6 -10 0 164.88 10.90 -6 -10 0 150.28 12.70 6 -10 0 149.49 12.50 -6 -10 0 162.78 12.20 6 -10 0 147.69 18.50 6 -10 0 185.88 14.40 -6 -10 0 153.48 14.20 6 -10 0 168.28 11.60 6 -10 0 175.08 12.10 -6 -10 0 174.88 18.70 6 -10 0 148.59 17.10 -6 -10 0 137.49 17.30 -6 -10 0 161.98 12.50 6 10 0 135.59 12.30 6 10 0 155.68 20.60 6 10 0 178.68 13.90 -7 -10 0 12.60 11.90 -7 -10 0 0.50 6.90 -7 -10 0 2.90 5.40 7 -10 0 -1.10 6.00 7 -10 0 8.30 7.40 -7 -10 0 -3.50 7.60 7 -10 0 0.10 6.20 -7 -10 0 0.90 6.00 7 -10 0 3.30 11.50 -7 -10 0 4.80 7.70 7 -10 0 0.20 7.10 7 -10 0 1.50 5.50 7 10 0 4.20 6.90 7 10 0 4.10 8.10 -7 10 0 7.70 5.20 7 10 0 -0.60 9.50 -7 10 0 8.80 12.50 -8 -10 0 33.70 14.40 -8 -10 0 21.00 9.30 -8 -10 0 20.70 7.20 8 -10 0 20.00 7.90 8 -10 0 32.60 11.20 -8 -10 0 23.30 9.20 8 -10 0 28.00 7.00 8 -10 0 20.10 14.40 -8 -10 0 10.80 10.50 8 -10 0 14.00 8.20 -8 -10 0 20.40 6.20 8 -10 0 27.30 8.50 8 10 0 16.20 9.50 -8 10 0 7.60 17.80 -8 10 0 23.10 7.20 8 10 0 9.00 14.50 8 10 0 17.60 7.60 -9 -10 0 0.30 9.10 9 -10 0 -1.80 9.10 9 -10 0 2.60 9.10 9 -10 0 9.90 7.50 9 -10 0 -0.40 8.00 -9 -10 0 1.30 5.70 -9 -10 0 -1.90 8.20 9 -10 0 -30.30 18.10 9 -10 0 2.00 11.70 -9 -10 0 -9.80 13.80 -9 10 0 -0.70 8.40 9 10 0 4.80 7.40 9 10 0 0.80 10.70 9 10 0 2.80 9.70 9 10 0 -16.50 16.60 -10 -10 0 42.60 19.30 10 -10 0 32.80 9.90 -10 -10 0 27.40 9.90 -10 -10 0 25.40 8.40 10 -10 0 24.80 7.90 10 -10 0 36.00 10.70 10 -10 0 35.60 9.90 10 -10 0 91.79 20.70 10 10 0 26.80 9.60 10 10 0 40.50 11.80 -10 10 0 29.70 11.50 -10 10 0 58.29 12.10 11 -10 0 13.30 10.10 11 -10 0 -17.90 9.60 -11 -10 0 -37.90 17.90 11 -10 0 -0.40 9.90 -11 -10 0 -0.90 9.10 11 -10 0 -1.30 7.20 -11 -10 0 -2.20 8.50 11 10 0 -6.90 10.50 -11 10 0 21.30 10.30 -11 10 0 -10.20 9.90 -11 10 0 -1.90 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5.00 4 -11 0 17.60 4.90 4 -11 0 12.80 5.00 -4 -11 0 13.50 8.20 -4 -11 0 20.90 4.70 -4 -11 0 13.80 7.90 4 -11 0 39.20 8.80 -4 -11 0 13.10 5.00 4 11 0 14.40 5.10 4 11 0 17.90 9.90 -5 -11 0 341.97 16.80 5 -11 0 310.57 16.80 5 -11 0 284.27 15.20 5 -11 0 316.27 19.40 -5 -11 0 307.07 14.90 5 -11 0 325.27 16.10 -5 -11 0 307.27 17.90 -5 -11 0 318.37 16.50 5 -11 0 282.37 20.90 -5 -11 0 308.37 20.80 -5 -11 0 339.97 23.10 -5 -11 0 312.17 16.60 5 -11 0 317.77 16.00 5 11 0 345.57 24.70 5 11 0 313.27 16.30 -6 -11 0 86.29 11.30 -6 -11 0 94.49 11.50 -6 -11 0 79.39 9.40 -6 -11 0 91.89 13.40 6 -11 0 129.59 10.20 6 -11 0 84.39 10.50 -6 -11 0 108.19 12.30 6 -11 0 92.99 15.60 6 -11 0 91.69 12.00 6 -11 0 88.39 17.70 6 -11 0 90.29 11.10 -6 -11 0 65.29 12.60 6 -11 0 79.79 11.30 -6 -11 0 93.49 17.90 6 11 0 111.69 20.10 6 11 0 66.99 11.20 6 11 0 109.39 13.10 -6 11 0 94.29 22.40 7 -11 0 132.19 13.20 7 -11 0 130.69 18.40 -7 -11 0 130.69 11.70 -7 -11 0 134.39 13.40 -7 -11 0 118.09 13.20 -7 -11 0 137.89 19.90 7 -11 0 155.78 13.60 -7 -11 0 131.79 15.60 -7 -11 0 145.19 14.60 7 -11 0 125.29 12.20 7 -11 0 129.09 12.90 -7 -11 0 148.59 21.20 7 -11 0 156.18 21.20 -7 11 0 86.29 22.40 7 11 0 130.59 13.40 7 11 0 126.09 16.20 -7 11 0 139.29 10.30 8 -11 0 17.20 8.30 -8 -11 0 -7.60 11.50 8 -11 0 23.00 7.10 8 -11 0 20.50 8.60 8 -11 0 31.40 15.70 8 -11 0 14.00 10.10 -8 -11 0 17.50 9.20 -8 -11 0 23.60 9.20 -8 -11 0 1.20 12.10 -8 -11 0 4.80 6.50 8 -11 0 12.50 7.80 -8 -11 0 12.80 7.80 8 11 0 3.20 9.20 8 11 0 4.30 7.70 8 11 0 37.90 16.90 -8 11 0 8.00 6.80 9 -11 0 96.39 14.40 -9 -11 0 78.29 10.40 9 -11 0 105.79 13.60 9 -11 0 117.49 20.10 9 -11 0 106.29 15.20 -9 -11 0 102.39 15.80 9 -11 0 95.69 15.20 -9 -11 0 94.59 16.20 -9 -11 0 59.89 24.80 9 11 0 61.19 12.80 9 11 0 71.79 16.40 -9 11 0 90.89 15.30 9 11 0 105.19 12.40 -10 -11 0 0.30 16.50 -10 -11 0 5.00 6.10 -10 -11 0 15.20 9.30 10 -11 0 9.70 7.40 10 -11 0 -19.30 9.40 10 -11 0 23.00 13.70 10 -11 0 -8.20 9.00 -10 -11 0 -1.50 9.30 10 -11 0 6.00 9.90 -10 11 0 25.10 11.80 10 11 0 -9.70 11.00 -10 11 0 -5.10 10.70 10 11 0 -9.60 8.80 11 -11 0 47.20 11.70 11 -11 0 101.69 21.00 -11 -11 0 77.99 15.60 -11 -11 0 66.39 14.10 11 -11 0 51.19 10.00 -11 11 0 98.69 17.10 -11 11 0 71.19 18.60 11 11 0 56.59 11.70 12 -11 0 1.60 7.90 12 -11 0 9.90 8.70 -12 -11 0 7.10 8.80 -12 -11 0 -0.40 7.40 12 -11 0 18.40 13.20 -12 11 0 19.30 8.30 12 11 0 -3.40 6.40 -12 11 0 10.60 9.30 0 -12 0 355.86 17.00 0 -12 0 386.96 20.40 0 -12 0 377.66 18.40 1 -12 0 1513.95 58.49 -1 -12 0 1476.45 56.39 -1 -12 0 1482.45 56.09 -1 -12 0 1484.65 59.19 1 -12 0 1473.35 56.09 1 -12 0 1526.35 56.29 -1 -12 0 1546.75 57.79 -1 12 0 1539.25 61.29 -2 -12 0 8.80 4.60 2 -12 0 11.70 4.80 -2 -12 0 11.40 6.50 2 -12 0 13.60 5.10 -2 -12 0 11.30 4.80 -2 -12 0 17.40 4.60 2 -12 0 18.10 7.20 -2 -12 0 10.40 5.60 -2 -12 0 6.10 6.40 2 -12 0 6.80 5.10 -2 12 0 8.10 6.80 2 12 0 18.80 7.60 -3 -12 0 257.17 15.10 3 -12 0 274.47 15.30 3 -12 0 269.77 13.60 -3 -12 0 262.47 14.70 3 -12 0 280.47 14.00 -3 -12 0 233.78 16.90 3 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0 32.30 8.20 6 -12 0 36.50 8.10 6 -12 0 48.20 11.60 6 -12 0 40.50 8.50 -6 -12 0 42.10 8.60 -6 -12 0 45.10 8.20 6 12 0 47.50 9.70 6 12 0 51.99 14.70 -6 12 0 23.60 14.10 6 12 0 28.80 7.60 -7 -12 0 -2.50 6.30 -7 -12 0 11.90 7.20 7 -12 0 6.70 7.10 7 -12 0 21.00 7.90 7 -12 0 6.50 7.40 -7 -12 0 7.20 8.50 -7 -12 0 3.70 7.00 -7 -12 0 -1.80 9.80 -7 -12 0 0.20 11.50 7 -12 0 12.50 7.90 -7 -12 0 13.30 11.50 7 -12 0 1.30 13.40 7 12 0 13.20 9.20 7 12 0 9.30 13.10 7 12 0 -2.20 7.40 -7 12 0 -33.20 15.60 8 -12 0 46.80 18.10 -8 -12 0 48.70 14.30 -8 -12 0 48.90 9.20 8 -12 0 36.00 9.00 8 -12 0 68.29 13.50 -8 -12 0 43.50 10.50 -8 -12 0 38.20 14.70 8 -12 0 45.20 11.30 -8 -12 0 43.30 9.70 8 -12 0 33.60 9.50 -8 -12 0 38.90 7.50 8 12 0 36.00 8.90 -8 12 0 39.30 7.60 8 12 0 38.30 18.80 8 12 0 51.19 10.90 -9 -12 0 21.00 11.50 -9 -12 0 0.40 14.10 9 -12 0 8.70 10.40 -9 -12 0 5.00 11.30 9 -12 0 5.10 14.50 9 -12 0 14.60 10.10 -9 -12 0 -1.20 11.00 9 -12 0 5.50 9.50 -9 12 0 7.00 9.00 9 12 0 -1.90 12.00 9 12 0 28.40 24.80 9 12 0 0.00 8.00 -10 -12 0 34.00 17.40 10 -12 0 26.60 11.90 10 -12 0 4.10 9.60 -10 -12 0 22.60 9.40 -10 -12 0 26.90 6.80 -10 -12 0 6.30 9.20 10 -12 0 -3.80 10.00 10 -12 0 3.80 9.80 10 12 0 11.60 10.80 10 12 0 13.50 9.70 -10 12 0 10.80 10.90 11 -12 0 87.89 19.10 11 -12 0 45.20 11.10 -11 -12 0 35.10 9.20 11 -12 0 50.79 10.10 -11 -12 0 47.00 9.20 11 12 0 27.40 7.10 -11 12 0 88.19 17.60 11 12 0 27.90 10.70 -11 12 0 46.90 11.10 12 -12 0 7.90 7.90 -12 -12 0 5.20 7.50 -12 -12 0 13.30 7.30 12 -12 0 8.60 8.00 12 -12 0 11.40 9.20 12 12 0 -4.20 7.40 -12 12 0 -5.80 8.30 12 12 0 6.30 6.30 -12 12 0 -9.40 7.50 0 -13 0 3.30 4.60 0 -13 0 -1.30 4.50 0 -13 0 -1.90 5.20 0 -13 0 5.50 5.00 0 -13 0 -7.60 5.20 0 -13 0 14.50 7.40 0 13 0 1.60 6.20 -1 -13 0 -0.40 4.00 1 -13 0 -3.90 5.00 1 -13 0 2.30 3.60 1 -13 0 1.70 4.70 -1 -13 0 13.20 7.00 1 -13 0 3.50 6.30 -1 -13 0 17.60 4.60 1 -13 0 13.20 5.00 -1 -13 0 12.00 4.40 -1 -13 0 2.00 5.80 -1 -13 0 3.10 6.90 -1 -13 0 -1.20 4.40 1 -13 0 0.80 4.10 -1 13 0 5.40 7.50 2 -13 0 66.89 8.60 -2 -13 0 84.19 8.40 2 -13 0 61.89 11.30 -2 -13 0 72.99 13.90 -2 -13 0 52.89 9.20 -2 -13 0 55.59 8.90 -2 -13 0 64.79 9.40 2 -13 0 86.69 9.80 2 -13 0 56.49 8.60 -2 -13 0 53.49 8.60 -2 -13 0 74.49 10.50 2 -13 0 68.19 8.00 2 13 0 93.49 16.60 -2 13 0 57.49 10.80 -3 -13 0 49.20 9.00 -3 -13 0 20.40 8.20 3 -13 0 33.90 8.80 3 -13 0 32.30 6.20 -3 -13 0 42.60 8.90 -3 -13 0 30.80 8.90 -3 -13 0 46.30 11.10 -3 -13 0 26.60 5.80 -3 -13 0 31.60 7.20 3 -13 0 32.40 5.50 -3 -13 0 32.10 6.90 3 -13 0 35.50 6.60 3 -13 0 62.49 9.50 3 -13 0 40.10 7.90 3 -13 0 38.50 5.70 -3 13 0 32.80 10.10 3 13 0 38.20 7.30 3 13 0 28.20 12.80 -4 -13 0 34.20 6.50 4 -13 0 41.10 10.10 4 -13 0 29.60 5.90 4 -13 0 53.29 9.00 4 -13 0 48.30 9.90 4 -13 0 30.40 7.30 -4 -13 0 43.90 7.90 -4 -13 0 45.90 8.20 -4 -13 0 30.70 10.50 4 -13 0 29.10 6.20 4 -13 0 34.30 6.40 -4 -13 0 25.30 8.80 -4 -13 0 58.79 9.20 -4 -13 0 17.30 7.20 -4 13 0 35.70 7.70 4 13 0 38.60 12.50 4 13 0 28.00 6.20 -4 13 0 26.40 11.10 -5 -13 0 9.30 10.90 5 -13 0 0.40 8.10 -5 -13 0 -2.50 7.80 5 -13 0 2.80 6.20 5 -13 0 -4.60 6.50 5 -13 0 5.10 6.30 5 -13 0 3.90 10.70 -5 -13 0 7.30 6.70 -5 -13 0 -3.90 9.80 -5 -13 0 2.50 5.90 5 -13 0 7.70 6.40 -5 -13 0 9.10 7.30 -5 -13 0 -8.10 9.60 5 13 0 8.30 11.40 -5 13 0 -9.70 10.90 5 13 0 1.90 6.50 -6 -13 0 150.68 14.60 -6 -13 0 147.29 22.20 -6 -13 0 148.39 16.60 6 -13 0 139.69 18.50 -6 -13 0 157.18 14.30 -6 -13 0 141.99 13.00 6 -13 0 137.49 14.10 -6 -13 0 134.69 13.90 6 -13 0 132.29 13.30 -6 -13 0 144.19 20.10 6 -13 0 117.69 22.10 6 -13 0 143.09 14.60 6 -13 0 158.98 13.00 6 13 0 170.38 17.50 6 13 0 126.49 13.70 7 -13 0 406.26 32.70 -7 -13 0 335.57 29.60 7 -13 0 343.17 20.40 7 -13 0 345.97 19.20 -7 -13 0 342.97 20.30 -7 -13 0 346.87 22.20 -7 -13 0 371.16 19.90 -7 -13 0 340.47 18.10 7 -13 0 364.86 20.20 -7 -13 0 335.57 19.80 -7 -13 0 364.56 28.10 7 -13 0 378.76 25.20 7 -13 0 349.67 19.70 7 13 0 334.47 19.70 7 13 0 341.37 32.50 7 13 0 347.57 23.00 -8 -13 0 33.00 7.80 -8 -13 0 25.70 10.10 8 -13 0 49.40 13.10 8 -13 0 26.70 9.80 8 -13 0 2.50 20.90 -8 -13 0 42.80 9.70 -8 -13 0 21.30 15.30 -8 -13 0 29.90 8.90 8 -13 0 25.00 8.00 8 -13 0 37.90 9.10 -8 13 0 31.20 7.80 8 13 0 28.50 8.80 8 13 0 35.70 11.00 8 13 0 -11.20 19.00 9 -13 0 1.70 9.50 -9 -13 0 -2.90 8.80 9 -13 0 16.60 8.60 -9 -13 0 8.50 7.10 9 -13 0 23.40 12.30 -9 -13 0 15.30 15.50 9 -13 0 8.40 9.60 -9 -13 0 -2.80 9.70 9 13 0 6.20 7.80 9 13 0 6.30 10.70 -9 13 0 13.50 9.20 9 13 0 -3.30 11.00 10 -13 0 -4.90 8.80 10 -13 0 22.50 11.60 10 -13 0 -5.20 9.20 -10 -13 0 -7.40 8.40 -10 -13 0 -17.80 16.70 -10 -13 0 -2.10 6.20 10 -13 0 -23.00 9.70 -10 -13 0 -0.90 9.20 10 13 0 -3.30 10.60 -10 13 0 -5.80 10.50 10 13 0 -1.90 9.50 11 -13 0 22.30 9.40 -11 -13 0 18.10 8.30 -11 -13 0 38.20 8.80 11 -13 0 15.30 8.60 11 -13 0 29.30 10.30 -11 13 0 68.69 16.90 11 13 0 27.80 9.90 -11 13 0 24.80 10.20 11 13 0 16.10 6.70 -12 -13 0 28.40 7.20 12 -13 0 30.20 8.90 12 -13 0 35.60 7.90 12 -13 0 25.10 7.40 12 13 0 15.60 6.20 -12 13 0 22.70 7.70 12 13 0 28.60 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310.67 22.40 5 -16 0 333.97 21.50 5 16 0 348.67 19.60 5 16 0 334.97 34.40 6 -16 0 206.28 20.50 -6 -16 0 228.68 24.70 -6 -16 0 230.48 18.00 6 -16 0 227.28 17.00 -6 -16 0 259.77 23.20 6 -16 0 213.98 16.50 -6 -16 0 225.98 16.50 6 -16 0 287.57 18.10 6 -16 0 239.18 16.20 -6 -16 0 204.48 17.30 -6 -16 0 226.78 29.50 -6 -16 0 230.18 16.30 6 16 0 216.98 34.70 6 16 0 276.17 22.40 6 16 0 233.88 17.70 -7 -16 0 45.10 12.50 -7 -16 0 38.70 14.70 -7 -16 0 39.00 9.10 7 -16 0 30.60 12.00 -7 -16 0 42.10 11.60 7 -16 0 31.90 13.70 -7 -16 0 42.70 16.40 7 -16 0 18.90 13.40 7 16 0 38.10 9.70 7 16 0 72.79 29.70 7 16 0 50.89 12.40 -8 -16 0 14.80 15.10 8 -16 0 -19.80 9.50 -8 -16 0 0.60 9.60 -8 -16 0 -8.80 7.60 8 -16 0 -0.40 10.90 -8 -16 0 5.50 8.10 8 -16 0 6.30 8.70 8 -16 0 3.70 7.70 -8 -16 0 -4.00 7.00 -8 16 0 0.10 7.30 8 16 0 8.90 10.90 8 16 0 4.60 10.40 8 16 0 -9.60 8.20 9 -16 0 -6.90 8.80 -9 -16 0 11.70 8.30 9 -16 0 6.90 10.40 9 -16 0 -7.80 7.70 9 -16 0 -9.10 8.20 -9 -16 0 -1.90 7.00 -9 -16 0 -3.00 8.70 9 16 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28.20 9.70 -11 2 2 24.30 8.60 11 2 -2 20.00 7.00 11 2 -2 31.70 18.60 -10 -2 2 16.90 6.10 10 -2 -2 30.10 9.30 -10 -2 2 5.60 13.10 10 -2 -2 30.70 12.80 10 -2 -2 23.30 8.40 10 -2 -2 29.30 9.20 -10 -2 2 20.60 7.50 -10 -2 2 20.80 8.30 -10 2 2 32.40 9.30 10 2 -2 15.10 6.90 10 2 -2 45.80 15.60 -10 2 2 20.90 8.20 -10 2 2 23.80 7.30 -10 2 2 12.80 12.50 10 2 -2 21.50 11.10 10 2 -2 24.10 10.20 9 -2 -2 2.10 7.20 -9 -2 2 5.20 7.00 -9 -2 2 4.90 5.30 9 -2 -2 3.40 9.80 9 -2 -2 5.80 6.60 9 -2 -2 10.10 11.80 -9 -2 2 4.00 6.20 9 -2 -2 10.00 8.30 -9 2 2 8.60 7.60 -9 2 2 1.40 5.70 9 2 -2 19.10 11.80 9 2 -2 -6.90 8.40 -9 2 2 -6.10 10.50 9 2 -2 3.30 6.60 9 2 -2 -1.70 8.80 -8 -2 2 64.19 9.50 -8 -2 2 48.00 7.30 8 -2 -2 46.30 7.70 -8 -2 2 31.70 9.90 8 -2 -2 46.20 10.90 8 -2 -2 44.90 9.00 8 -2 -2 46.00 10.50 -8 -2 2 49.50 8.60 8 -2 -2 32.30 9.20 8 2 -2 39.40 8.10 8 2 -2 48.70 7.40 8 2 -2 45.00 11.40 8 2 -2 49.10 6.90 -8 2 2 31.40 6.40 -8 2 2 40.90 10.00 7 -2 -2 5.80 6.70 -7 -2 2 8.70 3.60 7 -2 -2 -0.70 5.00 7 -2 -2 18.70 4.70 -7 -2 2 3.20 4.30 7 -2 -2 16.90 8.40 -7 -2 2 14.30 7.80 -7 2 2 6.10 4.70 -7 2 2 11.40 8.10 7 2 -2 10.00 7.10 7 2 -2 10.30 6.20 7 2 -2 18.00 4.40 6 -2 -2 53.59 10.80 -6 -2 2 46.70 7.70 6 -2 -2 35.00 9.40 -6 -2 2 44.80 7.40 -6 -2 2 37.20 7.70 -6 -2 2 35.30 5.60 -6 2 2 31.20 7.40 6 2 -2 30.90 7.50 6 2 -2 44.60 8.10 6 2 -2 39.30 4.50 6 2 -2 42.00 7.80 -6 2 2 37.50 6.30 -5 -2 2 1267.67 44.40 -5 -2 2 1241.98 46.10 -5 -2 2 1260.87 47.20 -5 -2 2 1148.49 47.30 5 -2 -2 1189.78 47.10 -5 -2 2 1251.17 45.50 5 -2 -2 1263.97 53.09 5 2 -2 1186.08 43.90 5 2 -2 1239.58 47.50 5 2 -2 1236.48 48.50 5 2 -2 1201.08 45.50 -5 2 2 1164.58 44.20 -5 2 2 1221.58 46.70 4 -2 -2 8.60 4.90 -4 -2 2 6.40 2.80 -4 -2 2 5.10 4.30 4 -2 -2 8.20 4.20 -4 -2 2 8.50 3.50 -4 -2 2 10.30 2.40 -4 2 2 10.10 3.50 4 2 -2 4.40 4.00 4 2 -2 8.80 4.30 4 2 -2 7.10 2.10 4 2 -2 10.60 2.90 -4 2 2 12.10 4.30 -4 2 2 7.20 2.10 3 -2 -2 2013.70 71.39 -3 -2 2 1896.31 69.59 3 -2 -2 2012.60 68.79 -3 -2 2 1830.62 68.19 -3 -2 2 1863.21 69.49 3 -2 -2 1981.60 69.19 -3 -2 2 1917.31 70.19 -3 2 2 1929.51 68.59 3 2 -2 1991.30 70.49 3 2 -2 2008.00 69.99 -3 2 2 1871.91 70.59 -3 2 2 1873.81 68.99 3 2 -2 1853.71 68.09 3 2 -2 1897.51 69.29 -2 -2 2 700.03 27.30 -2 -2 2 694.13 26.70 2 -2 -2 747.23 28.00 -2 -2 2 684.23 26.50 2 -2 -2 700.13 26.30 -2 2 2 760.12 28.90 2 2 -2 684.03 26.20 2 2 -2 700.63 26.90 -2 2 2 672.53 26.00 2 2 -2 706.03 26.60 -1 -2 2 605.84 22.40 1 -2 -2 583.74 22.10 -1 -2 2 564.44 22.90 -1 -2 2 588.74 21.70 1 -2 -2 582.34 22.90 1 2 -2 610.54 22.10 1 2 -2 559.54 22.70 1 2 -2 594.84 22.40 -1 2 2 567.14 22.10 -1 2 2 603.54 23.20 0 -2 2 3985.30 135.39 0 -2 -2 3808.02 134.89 0 -2 -2 3986.00 135.19 0 -2 2 3845.42 136.49 0 -2 -2 3712.73 135.89 0 -2 2 3859.21 135.19 0 2 -2 3738.23 136.19 0 2 -2 3799.52 135.69 0 2 -2 3749.02 135.39 0 2 2 3682.93 135.09 0 2 2 3980.80 134.89 0 2 2 3837.72 135.49 -1 -2 -2 25.90 4.50 1 -2 2 33.00 4.10 1 -2 2 28.00 5.20 -1 2 -2 25.00 3.90 1 2 2 28.20 4.40 1 2 2 32.20 4.80 -1 2 -2 31.10 3.80 -1 2 -2 20.80 4.00 -2 -2 -2 19.70 3.70 2 -2 2 17.30 3.50 2 -2 2 16.70 4.00 -2 2 -2 16.90 2.80 -2 2 -2 15.80 4.10 2 2 2 17.00 3.90 -2 2 -2 12.20 2.40 2 2 2 15.50 3.50 -3 -2 -2 130.09 7.00 -3 -2 -2 122.99 8.20 -3 -2 -2 130.19 8.40 3 -2 2 135.19 10.00 -3 2 -2 128.79 11.20 -3 2 -2 130.49 6.30 3 2 2 124.79 8.10 3 2 2 124.19 8.00 3 2 2 128.09 9.90 3 2 2 128.19 7.20 4 -2 2 36.10 6.90 -4 -2 -2 35.30 5.70 -4 -2 -2 18.00 4.60 -4 -2 -2 28.70 5.50 4 2 2 35.30 5.50 4 2 2 19.40 3.90 4 2 2 28.50 6.60 -4 2 -2 32.90 4.30 4 2 2 28.60 6.10 -5 -2 -2 483.65 21.80 -5 -2 -2 473.05 22.80 5 -2 2 509.55 25.20 -5 -2 -2 509.45 20.00 5 2 2 493.65 19.40 -5 2 -2 485.65 25.20 5 2 2 463.35 24.90 5 2 2 454.85 20.90 6 -2 2 60.69 13.70 -6 -2 -2 56.39 7.20 -6 -2 -2 69.19 10.00 6 -2 2 52.99 11.30 6 -2 2 59.69 6.70 -6 -2 -2 62.09 15.00 -6 -2 -2 57.39 7.90 6 2 2 48.80 5.60 6 2 2 56.89 7.90 -6 2 -2 54.59 7.10 6 2 2 64.59 11.00 -6 2 -2 63.49 13.90 6 2 2 42.30 9.90 -7 -2 -2 185.48 12.50 7 -2 2 146.49 19.80 7 -2 2 174.18 11.20 -7 -2 -2 184.68 11.10 7 -2 2 184.48 14.80 7 -2 2 180.08 11.80 7 -2 2 173.98 11.00 -7 -2 -2 206.18 15.20 -7 -2 -2 166.88 16.60 7 -2 2 196.18 16.80 7 2 2 178.28 16.30 -7 2 -2 216.18 13.20 -7 2 -2 181.88 12.80 7 2 2 186.58 11.50 7 2 2 186.18 20.40 -7 2 -2 179.98 11.90 -7 2 -2 171.68 21.60 8 -2 2 0.90 5.70 -8 -2 -2 17.50 5.30 8 -2 2 8.20 8.10 -8 -2 -2 16.10 11.00 8 -2 2 9.70 12.20 -8 -2 -2 15.20 6.70 8 -2 2 17.80 13.20 8 -2 2 12.40 5.70 -8 -2 -2 11.90 9.90 -8 2 -2 20.80 14.90 8 2 2 6.40 12.50 8 2 2 9.90 12.00 -8 2 -2 7.90 7.40 -8 2 -2 17.50 7.20 9 -2 2 19.00 8.90 -9 -2 -2 23.50 7.40 9 -2 2 20.70 7.10 -9 -2 -2 13.70 8.70 9 -2 2 15.70 7.20 9 -2 2 13.30 15.50 -9 -2 -2 29.10 13.10 9 -2 2 11.20 10.30 -9 2 -2 26.00 8.30 -9 2 -2 19.30 8.60 9 2 2 14.10 9.80 9 2 2 6.50 15.00 9 2 2 28.90 10.90 -10 -2 -2 93.19 17.70 -10 -2 -2 74.39 12.90 10 -2 2 55.29 12.20 10 -2 2 82.99 36.20 10 -2 2 74.99 11.70 10 -2 2 91.09 13.10 10 -2 2 70.89 16.00 -10 2 -2 56.59 10.50 -10 2 -2 51.09 10.70 10 2 2 91.09 19.90 -10 2 -2 83.09 12.40 10 2 2 59.19 11.90 11 -2 2 1.00 9.20 -11 -2 -2 7.10 9.00 11 -2 2 -7.00 13.00 -11 -2 -2 10.70 7.40 11 -2 2 17.40 8.20 11 -2 2 29.30 8.90 11 2 2 -0.50 11.80 11 2 2 5.30 9.10 -11 2 -2 -0.80 8.60 -11 2 -2 -3.00 10.00 12 -2 2 10.50 11.70 -12 -2 -2 8.10 9.40 12 -2 2 6.80 7.50 -12 -2 -2 18.70 8.00 12 2 2 13.00 8.40 -12 2 -2 15.90 8.70 12 2 2 -7.00 11.70 -12 2 -2 8.70 7.80 13 -2 2 19.00 6.70 -13 -2 -2 48.70 12.50 -13 -2 -2 28.00 8.20 13 -2 2 54.29 15.70 -13 2 -2 21.20 7.10 13 2 2 28.70 16.60 13 2 2 19.60 7.00 -14 -3 2 6.40 8.80 14 -3 -2 10.60 7.90 -14 -3 2 22.50 7.60 14 -3 -2 11.70 9.60 -14 3 2 4.60 9.10 14 3 -2 23.50 9.40 -14 3 2 12.50 8.60 -13 -3 2 42.50 10.90 -13 -3 2 30.10 8.30 13 -3 -2 46.00 12.20 13 -3 -2 37.40 9.30 13 -3 -2 33.10 10.30 -13 3 2 27.30 9.90 13 3 -2 80.79 17.70 13 3 -2 23.70 11.50 12 -3 -2 92.89 14.70 -12 -3 2 103.59 15.60 12 -3 -2 102.69 20.10 12 -3 -2 131.29 18.30 -12 -3 2 96.59 17.10 12 -3 -2 89.89 15.30 -12 -3 2 75.69 19.90 -12 -3 2 115.49 14.60 -12 3 2 80.29 15.00 -12 3 2 107.19 14.10 12 3 -2 83.79 12.10 -12 3 2 87.59 16.60 12 3 -2 74.19 18.00 12 3 -2 118.69 18.40 -11 -3 2 189.38 16.80 11 -3 -2 198.28 18.40 11 -3 -2 156.78 16.80 11 -3 -2 177.48 22.50 11 -3 -2 130.99 23.70 -11 -3 2 193.48 26.20 11 -3 -2 137.49 16.40 -11 -3 2 196.18 15.60 11 3 -2 168.68 22.10 -11 3 2 166.48 15.90 11 3 -2 116.89 21.90 -11 3 2 147.99 16.90 11 3 -2 199.08 19.50 11 3 -2 157.98 14.30 -11 3 2 181.88 18.40 10 -3 -2 49.40 10.70 10 -3 -2 45.20 9.10 -10 -3 2 39.60 8.10 -10 -3 2 44.20 13.30 10 -3 -2 41.70 12.70 10 -3 -2 40.00 15.30 -10 -3 2 71.49 14.80 10 -3 -2 96.29 16.70 10 3 -2 47.60 11.40 -10 3 2 37.20 8.70 -10 3 2 53.59 10.50 10 3 -2 40.30 15.00 10 3 -2 46.50 8.00 10 3 -2 40.30 11.20 -10 3 2 49.20 9.50 -10 3 2 34.40 12.90 9 -3 -2 222.08 21.60 9 -3 -2 226.48 16.70 -9 -3 2 231.78 22.30 -9 -3 2 232.08 14.40 -9 -3 2 230.38 15.80 9 -3 -2 247.58 17.00 9 -3 -2 233.78 14.70 9 -3 -2 235.88 23.70 -9 -3 2 232.68 12.60 9 3 -2 222.38 20.10 -9 3 2 237.88 16.10 9 3 -2 208.18 22.60 -9 3 2 197.98 20.50 9 3 -2 194.88 18.10 -9 3 2 296.37 17.50 8 -3 -2 34.60 6.90 8 -3 -2 39.40 7.20 -8 -3 2 37.20 7.20 8 -3 -2 37.60 9.80 8 -3 -2 47.40 11.20 8 -3 -2 34.70 6.10 -8 -3 2 41.20 8.30 -8 -3 2 28.10 6.00 8 -3 -2 49.00 10.80 -8 -3 2 40.80 11.10 8 3 -2 40.70 10.40 -8 3 2 32.20 7.10 8 3 -2 24.80 10.30 -8 3 2 33.30 10.10 8 3 -2 36.60 8.20 8 3 -2 34.90 8.00 7 -3 -2 400.06 22.30 -7 -3 2 374.06 17.80 -7 -3 2 364.06 18.60 7 -3 -2 368.66 17.60 7 -3 -2 372.46 17.10 7 -3 -2 377.86 20.30 -7 -3 2 359.86 21.40 7 -3 -2 354.66 16.50 -7 -3 2 364.86 16.10 7 3 -2 383.46 18.90 7 3 -2 394.36 32.80 7 3 -2 345.47 15.00 -7 3 2 349.96 20.20 7 3 -2 367.56 16.70 -7 3 2 383.26 16.80 -6 -3 2 200.08 12.20 -6 -3 2 184.68 12.80 -6 -3 2 201.78 14.70 -6 -3 2 170.88 10.40 6 -3 -2 184.58 14.80 -6 3 2 174.88 9.70 6 3 -2 189.48 9.10 6 3 -2 188.18 14.50 6 3 -2 213.48 16.50 -6 3 2 181.28 13.70 5 -3 -2 56.19 12.70 -5 -3 2 55.09 7.50 -5 -3 2 33.40 7.70 5 -3 -2 43.70 8.70 -5 -3 2 53.49 7.30 -5 -3 2 54.99 9.10 -5 -3 2 51.39 5.10 5 3 -2 51.09 6.70 5 3 -2 56.89 5.10 5 3 -2 53.09 9.10 -5 3 2 53.69 4.50 -5 3 2 67.39 8.60 5 3 -2 48.50 9.60 -4 -3 2 119.69 8.40 -4 -3 2 123.99 9.30 -4 -3 2 123.39 8.80 4 -3 -2 133.49 12.50 4 -3 -2 117.69 8.90 -4 -3 2 115.49 6.10 -4 3 2 106.89 10.10 4 3 -2 123.49 9.80 -4 3 2 118.49 8.70 4 3 -2 117.69 6.20 4 3 -2 102.39 9.80 4 3 -2 118.39 7.70 -3 -3 2 161.68 8.90 3 -3 -2 156.08 11.10 -3 -3 2 142.19 8.60 3 -3 -2 145.89 8.30 3 3 -2 163.98 10.00 -3 3 2 137.79 6.90 3 3 -2 148.89 9.60 3 3 -2 143.19 6.80 3 3 -2 143.09 8.20 -3 3 2 145.79 9.50 2 -3 -2 118.39 8.60 -2 -3 2 119.59 7.00 -2 -3 2 118.89 7.10 -2 -3 2 105.69 7.50 2 -3 -2 110.49 6.10 -2 3 2 109.99 7.40 -2 3 2 106.59 6.10 2 3 -2 119.19 7.10 -2 3 2 104.39 5.90 2 3 -2 110.59 6.70 -1 -3 2 40.10 4.90 -1 -3 2 33.90 4.10 1 -3 -2 32.90 4.60 1 -3 -2 34.10 5.80 -1 -3 2 32.50 5.70 1 3 -2 32.20 6.20 -1 3 2 42.50 5.60 -1 3 2 36.00 4.70 0 -3 -2 3805.42 136.29 0 -3 2 4022.60 136.29 0 -3 2 3799.82 136.19 0 -3 -2 3715.73 135.99 0 3 2 3885.61 136.09 0 3 -2 4001.50 136.49 0 3 -2 3838.42 137.39 0 3 -2 3687.83 136.59 0 3 2 3927.41 135.99 -1 -3 -2 1338.17 51.19 1 -3 2 1510.75 50.89 -1 -3 -2 1401.66 51.39 -1 -3 -2 1322.97 51.79 1 -3 2 1423.96 52.49 -1 3 -2 1470.05 53.29 -1 3 -2 1347.07 51.39 1 3 2 1485.75 51.69 -2 -3 -2 304.97 13.70 -2 -3 -2 299.57 13.40 2 -3 2 309.27 12.10 2 -3 2 304.87 14.30 2 3 2 289.17 13.80 -2 3 -2 294.27 11.50 2 3 2 298.97 12.30 2 3 2 311.97 14.60 -2 3 -2 312.47 12.10 -2 3 -2 311.77 16.10 -3 -3 -2 314.87 14.60 3 -3 2 318.67 16.00 -3 -3 -2 304.77 14.40 -3 3 -2 303.37 12.20 3 3 2 312.37 14.80 3 3 2 329.07 16.30 -3 3 -2 285.37 24.00 3 3 2 318.07 13.40 4 -3 2 303.87 17.10 -4 -3 -2 302.47 12.60 -4 -3 -2 302.57 15.00 -4 3 -2 292.27 12.40 4 3 2 298.97 14.90 4 3 2 318.97 17.80 4 3 2 277.57 14.60 4 3 2 292.87 13.30 -5 -3 -2 81.79 9.70 -5 -3 -2 80.09 6.50 5 -3 2 69.09 12.60 -5 3 -2 63.19 12.80 -5 3 -2 78.09 6.50 5 3 2 73.19 8.70 5 3 2 78.89 13.40 5 3 2 77.69 7.30 -6 -3 -2 63.49 6.80 6 -3 2 50.69 7.20 -6 -3 -2 80.89 10.80 6 -3 2 57.99 6.80 6 -3 2 59.39 8.30 6 -3 2 65.59 11.70 -6 -3 -2 64.99 13.20 -6 3 -2 64.49 7.40 -6 3 -2 78.09 15.00 6 3 2 72.59 14.60 6 3 2 71.99 9.90 6 3 2 58.29 11.70 6 3 2 64.89 10.80 7 -3 2 92.79 9.20 -7 -3 -2 86.99 9.60 -7 -3 -2 96.19 8.20 7 -3 2 98.49 9.30 7 -3 2 95.29 14.40 -7 -3 -2 99.09 13.70 7 -3 2 67.19 13.70 7 -3 2 78.79 8.80 -7 -3 -2 75.79 7.20 7 -3 2 77.79 12.70 -7 -3 -2 107.79 12.90 7 3 2 96.49 10.60 -7 3 -2 81.59 19.40 7 3 2 90.09 13.30 -7 3 -2 86.59 10.10 -7 3 -2 90.19 9.30 7 3 2 62.69 13.80 8 -3 2 15.80 7.90 8 -3 2 23.30 14.00 -8 -3 -2 30.20 6.60 8 -3 2 21.20 6.30 8 -3 2 22.70 7.50 -8 -3 -2 29.80 8.30 -8 -3 -2 33.00 12.10 8 -3 2 28.10 10.80 -8 -3 -2 25.60 5.80 8 -3 2 16.10 6.70 8 3 2 27.70 8.10 -8 3 -2 31.60 8.10 -8 3 -2 45.10 16.80 8 3 2 29.60 15.30 8 3 2 34.50 10.30 -8 3 -2 36.00 7.50 -9 -3 -2 256.97 15.70 -9 -3 -2 304.17 22.40 9 -3 2 244.58 18.50 9 -3 2 255.67 24.30 -9 -3 -2 247.68 19.80 9 -3 2 230.18 28.90 9 -3 2 249.88 15.70 9 -3 2 239.88 16.80 -9 3 -2 276.67 18.40 9 3 2 264.97 21.20 -9 3 -2 359.86 56.19 9 3 2 273.77 30.50 9 3 2 260.57 22.10 -9 3 -2 253.57 18.20 10 -3 2 -1.00 23.60 10 -3 2 -11.20 7.40 10 -3 2 13.60 12.00 -10 -3 -2 16.80 10.00 10 -3 2 0.50 8.10 10 -3 2 11.70 8.80 -10 -3 -2 1.80 7.20 -10 3 -2 -18.40 11.20 -10 3 -2 -3.10 8.00 10 3 2 5.60 11.40 10 3 2 21.30 24.00 10 3 2 2.90 10.50 -10 3 -2 4.30 9.60 -11 -3 -2 17.50 9.50 11 -3 2 14.50 8.70 11 -3 2 -3.70 8.40 -11 -3 -2 22.60 11.00 11 -3 2 1.50 13.30 11 -3 2 2.80 8.20 -11 3 -2 14.30 7.80 -11 3 -2 3.50 9.40 -11 3 -2 0.60 10.30 11 3 2 15.50 9.70 11 3 2 11.80 11.60 12 -3 2 12.10 7.90 12 -3 2 9.40 12.10 -12 -3 -2 59.49 15.40 -12 -3 -2 13.10 9.50 -12 3 -2 22.90 9.20 12 3 2 21.10 8.70 -12 3 -2 6.40 8.20 12 3 2 4.60 11.70 13 -3 2 52.49 10.70 -13 -3 -2 27.60 7.80 13 -3 2 30.90 9.70 -13 -3 -2 59.59 12.40 13 3 2 53.59 11.90 -13 3 -2 33.40 9.20 13 3 2 21.30 8.60 -14 -4 2 35.50 8.70 -14 -4 2 23.50 7.70 14 -4 -2 21.20 7.80 14 -4 -2 32.00 9.70 14 4 -2 69.39 13.40 -14 4 2 36.20 8.60 13 -4 -2 9.70 8.50 -13 -4 2 2.10 7.60 13 -4 -2 21.20 13.50 13 -4 -2 29.70 11.90 -13 -4 2 12.10 9.40 13 4 -2 30.70 9.80 13 4 -2 -18.30 9.30 -13 4 2 10.70 9.40 -13 4 2 0.70 8.60 12 -4 -2 85.09 21.00 12 -4 -2 57.49 11.20 -12 -4 2 42.50 9.60 -12 -4 2 48.60 11.60 12 -4 -2 35.80 10.50 12 -4 -2 46.50 10.10 -12 -4 2 42.40 19.60 12 4 -2 40.70 11.50 12 4 -2 59.29 11.30 -12 4 2 25.40 8.90 -12 4 2 41.70 9.60 12 4 -2 75.09 17.80 -12 4 2 44.80 10.70 11 -4 -2 40.80 12.60 11 -4 -2 24.80 10.20 11 -4 -2 23.00 10.00 -11 -4 2 32.50 9.60 11 -4 -2 27.50 9.70 -11 -4 2 18.50 7.50 11 -4 -2 68.49 27.60 -11 -4 2 31.00 11.10 -11 -4 2 7.70 16.10 11 4 -2 30.70 18.10 -11 4 2 10.40 10.10 -11 4 2 14.80 9.00 -11 4 2 20.70 10.40 11 4 -2 41.20 8.20 11 4 -2 24.20 10.00 10 -4 -2 -1.00 12.30 -10 -4 2 11.00 14.60 10 -4 -2 15.50 9.90 10 -4 -2 10.40 15.50 -10 -4 2 10.90 7.00 10 -4 -2 27.70 8.90 10 -4 -2 14.10 8.40 -10 -4 2 13.50 8.50 10 4 -2 37.80 15.90 -10 4 2 23.50 13.90 10 4 -2 17.50 9.50 -10 4 2 13.70 9.40 -10 4 2 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4 -3.70 9.10 6 -13 -4 4.90 5.50 6 -13 -4 6.10 9.40 -6 -13 4 11.40 12.00 6 13 -4 32.20 9.90 6 13 -4 -8.40 12.70 6 13 -4 -2.70 6.30 5 -13 -4 24.40 7.40 5 -13 -4 22.90 6.30 -5 -13 4 16.60 11.10 5 -13 -4 25.50 7.40 5 -13 -4 16.00 9.80 5 -13 -4 5.90 5.50 -5 -13 4 12.50 6.30 -5 -13 4 7.40 6.70 5 -13 -4 9.70 6.30 -5 -13 4 17.20 9.10 -5 -13 4 15.30 10.60 5 -13 -4 16.60 7.60 -5 -13 4 14.80 6.50 -5 -13 4 12.80 7.10 5 13 -4 6.80 11.90 -5 13 4 20.80 8.50 5 13 -4 11.10 6.00 4 -13 -4 109.79 15.60 4 -13 -4 132.79 13.00 -4 -13 4 113.19 11.20 -4 -13 4 127.89 14.60 4 -13 -4 113.29 10.20 -4 -13 4 118.69 12.20 4 -13 -4 129.99 11.90 -4 -13 4 122.09 19.90 -4 -13 4 134.59 10.60 -4 -13 4 137.69 20.40 -4 -13 4 130.39 14.30 -4 -13 4 125.69 14.70 4 -13 -4 131.19 12.20 4 -13 -4 122.49 11.70 4 13 -4 132.39 10.80 -4 13 4 153.08 15.30 4 13 -4 98.39 17.00 3 -13 -4 207.18 15.60 -3 -13 4 253.77 14.30 -3 -13 4 270.47 21.80 3 -13 -4 257.17 18.70 -3 -13 4 219.98 12.70 -3 -13 4 227.18 13.90 3 -13 -4 231.48 14.30 -3 -13 4 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29.70 9.50 -2 -14 4 25.80 6.20 2 -14 -4 26.70 8.50 -2 -14 4 22.40 7.00 2 -14 -4 22.20 5.80 2 -14 -4 30.10 7.30 2 -14 -4 19.10 6.90 -2 -14 4 17.90 6.30 -2 -14 4 22.30 6.60 -2 -14 4 19.00 6.90 -2 14 4 9.00 8.50 2 14 -4 24.40 4.90 -2 14 4 3.10 8.80 2 14 -4 20.20 10.40 -1 -14 4 -3.00 6.50 -1 -14 4 -7.40 7.30 -1 -14 4 8.90 5.70 -1 -14 4 3.20 6.70 1 -14 -4 2.70 6.20 -1 -14 4 1.10 5.50 -1 -14 4 -0.40 7.10 -1 -14 4 -2.20 5.50 1 -14 -4 11.00 4.90 1 -14 -4 4.00 5.30 1 -14 -4 0.50 5.90 1 -14 -4 2.30 6.00 1 -14 -4 5.50 8.20 1 14 -4 2.30 3.80 1 14 -4 -0.80 9.40 -1 14 4 10.00 7.80 -1 14 4 -3.10 9.60 0 -14 -4 8.10 4.90 0 -14 4 13.80 7.10 0 -14 -4 32.20 10.00 0 -14 4 15.40 6.60 0 -14 -4 17.90 6.30 0 -14 -4 7.00 6.00 0 -14 4 13.90 8.50 0 -14 4 10.10 6.70 0 -14 -4 13.60 7.50 0 -14 4 15.40 5.50 0 -14 4 14.70 6.50 0 -14 -4 12.80 7.00 0 14 -4 17.40 11.60 0 14 4 27.70 9.60 0 14 4 20.80 11.40 -1 -14 -4 26.80 6.50 -1 -14 -4 23.00 7.70 -1 -14 -4 10.40 9.10 1 -14 4 25.20 6.30 1 -14 4 20.70 5.30 1 -14 4 9.50 6.60 1 -14 4 23.10 6.60 1 -14 4 26.70 7.40 -1 -14 -4 28.30 7.80 -1 -14 -4 17.00 6.90 1 -14 4 21.40 9.80 -1 -14 -4 29.30 10.70 1 -14 4 18.70 7.00 -1 -14 -4 23.20 6.70 -1 14 -4 25.30 12.50 1 14 4 17.40 10.10 1 14 4 26.90 12.00 1 14 4 9.10 4.50 2 -14 4 288.17 19.50 2 -14 4 299.07 15.70 2 -14 4 316.17 17.50 -2 -14 -4 292.67 17.70 2 -14 4 304.67 18.90 -2 -14 -4 310.07 22.40 -2 -14 -4 321.97 18.10 2 -14 4 306.87 18.80 -2 -14 -4 301.77 23.60 -2 -14 -4 332.27 17.30 -2 -14 -4 325.47 18.30 2 -14 4 309.27 16.40 -2 14 -4 305.87 30.10 2 14 4 297.07 16.50 2 14 4 299.47 24.40 2 14 4 311.97 25.40 3 -14 4 143.29 12.20 -3 -14 -4 143.29 14.70 -3 -14 -4 148.09 17.80 3 -14 4 161.38 15.00 -3 -14 -4 160.78 15.50 3 -14 4 137.09 11.90 3 -14 4 162.18 14.30 3 -14 4 172.28 14.10 -3 -14 -4 131.19 18.90 -3 -14 -4 144.69 13.20 -3 -14 -4 155.38 14.70 3 14 4 166.18 27.90 3 14 4 166.18 13.80 3 14 4 149.49 23.80 -3 14 -4 141.79 29.50 4 -14 4 99.99 14.00 4 -14 4 63.49 13.10 -4 -14 -4 58.69 14.00 -4 -14 -4 78.09 12.30 4 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12 10 15.00 7.00 6 12 -10 16.40 5.80 6 12 -10 9.50 7.30 6 12 -10 14.40 5.90 5 -12 -10 104.99 19.80 -5 -12 10 100.09 14.60 -5 -12 10 81.39 11.10 -5 -12 10 121.49 15.40 -5 -12 10 104.99 19.90 5 -12 -10 107.79 16.60 5 -12 -10 83.79 17.90 5 -12 -10 60.79 11.30 -5 -12 10 84.59 11.00 5 -12 -10 91.89 15.20 5 12 -10 96.19 18.70 5 12 -10 76.69 9.90 -5 12 10 114.39 12.70 5 12 -10 106.29 10.30 5 12 -10 93.09 12.10 -4 -12 10 7.30 8.60 4 -12 -10 4.10 8.30 4 -12 -10 2.20 10.20 4 -12 -10 -0.20 14.00 -4 -12 10 -0.20 6.10 -4 -12 10 5.80 5.70 -4 -12 10 14.00 7.20 4 -12 -10 -2.20 9.80 -4 -12 10 1.30 7.60 -4 -12 10 5.90 9.00 4 -12 -10 -2.90 9.20 4 12 -10 6.70 5.50 -4 12 10 11.40 7.00 4 12 -10 -0.40 15.00 4 12 -10 11.10 6.50 -3 -12 10 288.97 25.20 3 -12 -10 287.27 28.70 3 -12 -10 292.27 21.20 -3 -12 10 308.17 18.60 -3 -12 10 287.77 16.60 -3 -12 10 281.47 16.60 3 -12 -10 304.97 23.40 3 -12 -10 310.87 19.80 -3 -12 10 301.47 18.80 -3 -12 10 305.47 18.80 3 -12 -10 301.47 15.30 3 12 -10 285.07 16.80 -3 12 10 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8.30 2 -10 -15 27.00 10.50 -2 -10 15 21.80 7.70 -2 -10 15 25.80 7.90 2 -10 -15 20.60 6.00 2 -10 -15 9.80 9.60 -2 10 15 9.10 9.80 2 10 -15 23.90 5.50 -2 10 15 19.40 8.10 -2 10 15 24.20 8.60 2 10 -15 22.60 7.10 1 -10 -15 97.29 17.50 1 -10 -15 119.99 10.40 -1 -10 15 114.89 11.70 1 -10 -15 108.89 14.80 -1 -10 15 115.99 12.70 1 -10 -15 123.19 13.20 -1 10 15 80.99 16.10 1 10 -15 134.99 11.30 1 10 -15 143.29 10.10 -1 10 15 147.79 14.70 1 10 -15 91.19 11.90 0 -10 -15 26.80 8.30 0 -10 -15 27.20 10.20 0 -10 15 32.60 7.40 0 -10 15 34.10 6.40 0 10 -15 28.40 5.80 0 10 -15 46.50 8.60 0 10 15 27.10 8.90 -1 -10 -15 188.58 17.70 -1 -10 -15 185.38 11.40 1 -10 15 191.88 12.70 1 -10 15 138.99 10.00 -1 10 -15 206.38 12.00 1 10 15 181.48 14.00 1 10 15 177.78 20.00 -2 -10 -15 1.50 5.00 2 -10 15 4.10 5.60 -2 10 -15 0.10 4.40 2 10 15 -3.80 8.10 -11 -11 15 28.30 6.80 11 -11 -15 30.90 7.30 11 -11 -15 29.60 11.10 11 -11 -15 30.30 7.90 11 11 -15 35.30 7.70 11 11 -15 38.20 7.80 -11 11 15 29.90 7.30 -10 -11 15 18.00 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-18 0.20 4.40 4 -3 -18 52.59 8.60 -4 -3 18 76.69 12.40 4 3 -18 59.69 7.50 -4 3 18 58.69 11.30 4 3 -18 45.90 7.40 3 -3 -18 44.90 6.60 3 -3 -18 52.29 10.20 -3 -3 18 67.79 10.60 3 3 -18 35.70 8.10 3 3 -18 53.19 7.20 -3 3 18 70.69 10.80 -3 3 18 67.19 12.80 -2 -3 18 10.90 6.20 2 -3 -18 1.60 6.00 2 -3 -18 1.30 4.10 2 3 -18 4.20 4.30 -2 3 18 6.80 5.90 -2 3 18 6.80 6.70 -1 -3 18 30.20 6.40 -1 3 18 30.70 6.20 10 -4 -18 22.20 6.00 -10 -4 18 34.20 6.30 -10 -4 18 23.80 5.00 10 4 -18 30.70 5.20 -10 4 18 34.60 6.80 10 4 -18 34.40 6.30 -9 -4 18 4.10 5.30 9 -4 -18 4.40 5.80 -9 -4 18 -6.40 5.00 9 -4 -18 9.80 6.00 -9 4 18 5.00 5.70 9 4 -18 6.80 6.30 -9 4 18 8.20 6.50 9 4 -18 20.30 8.20 8 -4 -18 5.30 5.90 8 -4 -18 -0.60 5.50 -8 -4 18 9.60 5.70 -8 -4 18 1.50 5.80 -8 4 18 8.00 5.60 8 4 -18 0.00 6.50 -8 4 18 -0.70 6.50 -7 -4 18 2.30 5.80 7 -4 -18 -0.40 6.70 -7 -4 18 9.20 5.90 7 -4 -18 0.50 6.00 7 4 -18 4.80 6.30 -7 4 18 6.00 6.50 -7 4 18 9.00 5.10 6 -4 -18 7.80 6.50 -6 -4 18 9.00 4.60 -6 -4 18 24.80 6.60 6 -4 -18 20.40 6.10 -6 4 18 22.40 5.30 -6 4 18 16.50 7.10 6 4 -18 12.50 6.80 -5 -4 18 -4.30 6.00 -5 -4 18 -11.00 4.40 5 -4 -18 4.10 6.80 -5 4 18 5.10 6.50 5 4 -18 -2.70 4.10 5 4 -18 -2.00 6.10 4 -4 -18 60.69 10.80 -4 -4 18 71.19 10.70 4 4 -18 73.29 10.30 4 4 -18 55.19 7.10 -4 4 18 69.49 11.00 3 -4 -18 3.60 6.50 -3 -4 18 6.60 6.10 3 -4 -18 5.00 6.30 -3 4 18 6.80 6.60 3 4 -18 4.70 4.20 3 4 -18 17.00 5.90 -3 4 18 11.50 7.20 2 -4 -18 19.50 4.50 -2 -4 18 25.20 6.20 2 -4 -18 23.40 6.30 -2 4 18 22.50 7.70 2 4 -18 28.70 6.40 -2 4 18 18.40 6.10 9 -5 -18 5.60 6.00 -9 -5 18 7.30 5.50 9 -5 -18 -0.90 5.70 -9 -5 18 2.50 5.60 -9 5 18 8.90 5.80 9 5 -18 1.50 5.70 -9 5 18 13.70 6.50 8 -5 -18 -4.40 5.70 8 -5 -18 -0.10 7.00 -8 -5 18 -0.70 5.40 -8 -5 18 -3.70 5.20 -8 5 18 -1.10 6.40 8 5 -18 -4.50 6.00 -8 5 18 7.20 5.50 -7 -5 18 31.70 6.40 7 -5 -18 26.60 6.60 -7 -5 18 32.30 6.40 7 -5 -18 27.90 7.40 -7 5 18 33.70 6.60 -7 5 18 52.29 9.80 7 5 -18 30.60 6.90 -6 -5 18 1.80 4.60 6 -5 -18 7.30 6.70 -6 -5 18 -1.40 5.70 6 -5 -18 -6.20 5.10 6 5 -18 -8.40 6.00 -6 5 18 4.60 6.60 -6 5 18 6.10 5.40 5 -5 -18 25.50 7.10 -5 -5 18 30.70 5.30 -5 -5 18 28.50 6.60 -5 5 18 46.50 8.60 5 5 -18 32.40 6.50 5 5 -18 20.80 5.70 -5 5 18 26.80 7.20 -4 -5 18 16.70 6.50 4 -5 -18 26.10 8.30 4 5 -18 18.00 4.30 4 5 -18 22.40 7.20 -4 5 18 17.80 6.70 -3 -5 18 1.20 5.70 3 -5 -18 -12.10 8.90 -3 5 18 5.10 7.50 3 5 -18 8.40 5.30 3 5 -18 5.10 3.90 -3 5 18 0.80 6.00 2 -5 -18 32.00 6.90 2 -5 -18 26.40 5.80 -2 -5 18 40.60 8.50 -2 5 18 41.90 6.30 -2 5 18 54.69 11.70 2 5 -18 36.40 6.20 9 -6 -18 -6.70 5.90 9 -6 -18 3.00 5.70 -9 -6 18 -2.50 5.30 -9 -6 18 -6.40 4.40 9 6 -18 -0.10 5.30 -9 6 18 6.60 6.10 -9 6 18 10.10 5.40 8 -6 -18 31.80 6.20 8 -6 -18 26.50 6.50 -8 -6 18 37.60 7.90 -8 -6 18 33.90 6.50 -8 6 18 33.90 7.00 8 6 -18 25.20 8.00 -8 6 18 46.50 9.60 7 -6 -18 11.10 7.20 7 -6 -18 3.80 5.80 -7 -6 18 0.50 5.10 -7 -6 18 2.30 5.20 -7 6 18 1.40 5.50 -7 6 18 0.20 5.90 7 6 -18 -0.40 5.70 6 -6 -18 10.70 7.10 -6 -6 18 7.60 5.80 -6 -6 18 3.70 5.80 6 -6 -18 0.60 5.50 -6 6 18 7.10 5.60 6 6 -18 0.70 6.10 -6 6 18 4.70 6.30 -5 -6 18 10.60 4.60 -5 -6 18 19.70 5.90 5 -6 -18 4.10 7.00 -5 6 18 21.60 5.80 5 6 -18 15.10 5.90 -5 6 18 13.50 6.60 5 6 -18 9.80 5.60 4 -6 -18 56.19 11.00 -4 -6 18 48.80 9.00 -4 -6 18 31.00 6.00 4 6 -18 37.60 6.30 -4 6 18 37.20 7.10 -4 6 18 56.19 8.40 4 6 -18 36.50 6.30 -3 -6 18 6.00 5.50 3 -6 -18 9.30 6.20 -3 6 18 2.50 5.40 3 6 -18 6.10 5.10 3 6 -18 2.30 3.70 -2 -6 18 3.90 5.30 -2 6 18 5.40 4.70 -8 -7 18 1.50 5.30 8 -7 -18 2.90 5.80 -8 -7 18 -0.20 4.40 8 -7 -18 -0.90 5.40 8 7 -18 6.80 5.60 -8 7 18 -2.20 5.80 -8 7 18 5.70 5.40 -7 -7 18 -0.50 4.80 7 -7 -18 -13.90 5.30 -7 -7 18 -4.80 4.60 7 -7 -18 -4.40 5.60 7 7 -18 -5.10 8.50 -7 7 18 0.50 5.50 -7 7 18 -1.50 5.90 6 -7 -18 6.40 6.00 6 -7 -18 2.80 7.50 -6 -7 18 8.40 5.30 -6 -7 18 8.20 4.90 -6 7 18 17.00 5.70 6 7 -18 12.50 7.80 -6 7 18 11.50 6.30 -5 -7 18 -3.90 4.30 5 -7 -18 -6.40 8.40 -5 -7 18 0.30 5.10 5 -7 -18 -9.80 6.20 -5 7 18 8.80 5.20 -5 7 18 -1.50 5.80 5 7 -18 -0.50 3.50 5 7 -18 3.50 5.10 -4 -7 18 -2.10 5.20 4 -7 -18 4.10 8.10 -4 -7 18 -4.10 3.60 -4 7 18 -0.40 5.30 -4 7 18 4.20 5.00 4 7 -18 -6.00 5.00 4 7 -18 -3.70 3.80 3 -7 -18 7.70 6.00 -3 -7 18 2.90 5.00 3 7 -18 3.80 7.60 -3 7 18 3.80 5.80 3 7 -18 0.90 3.60 8 -8 -18 -2.10 5.50 8 -8 -18 1.70 5.40 8 8 -18 2.50 5.20 7 -8 -18 26.70 6.00 -7 -8 18 25.20 5.10 -7 -8 18 28.60 5.50 -7 8 18 43.80 9.50 7 8 -18 37.70 6.20 -7 8 18 34.40 6.10 -6 -8 18 -0.30 4.80 6 -8 -18 5.40 6.30 -6 -8 18 0.10 4.50 6 -8 -18 5.00 5.80 -6 8 18 11.40 6.30 -6 8 18 6.90 5.50 6 8 -18 0.10 5.10 5 -8 -18 16.30 6.40 -5 -8 18 22.40 5.00 -5 -8 18 25.90 5.20 5 -8 -18 30.90 5.20 -5 8 18 30.50 6.10 -5 8 18 42.60 8.90 5 8 -18 16.50 3.90 5 8 -18 26.70 5.90 4 -8 -18 13.20 6.60 -4 -8 18 3.40 3.70 -4 -8 18 12.90 5.00 4 8 -18 13.50 5.00 -4 8 18 8.80 5.30 4 8 -18 8.40 5.80 -4 8 18 14.50 5.10 6 -9 -18 3.40 5.50 -6 -9 18 -0.10 4.70 -6 -9 18 0.80 3.80 6 -9 -18 5.30 6.40 6 9 -18 -2.90 4.90 -6 9 18 -1.00 5.20 -6 9 18 2.60 5.40 -8 0 19 1.60 5.50 8 0 -19 -5.90 4.90 7 0 -19 5.20 5.90 -7 0 19 11.00 5.60 6 0 -19 3.50 5.40 -6 0 19 -3.00 5.30 -5 0 19 6.60 5.70 4 0 -19 0.30 4.90 -4 0 19 0.10 5.20 -7 -1 19 28.30 6.10 7 -1 -19 24.90 6.00 7 1 -19 23.60 6.20 -7 1 19 34.60 5.90 6 -1 -19 4.50 5.20 -6 -1 19 4.10 5.30 6 1 -19 0.60 6.20 -6 1 19 9.20 5.50 5 -1 -19 19.30 5.50 -5 -1 19 22.40 5.80 5 1 -19 15.30 5.20 -5 1 19 19.80 6.00 -4 -1 19 52.89 8.50 -7 -2 19 3.10 5.20 7 -2 -19 0.20 5.60 7 2 -19 7.20 5.60 -7 2 19 -0.10 5.20 -6 -2 19 23.60 5.90 6 -2 -19 14.10 6.00 6 2 -19 25.80 6.10 -6 2 19 26.60 6.00 -5 -2 19 2.40 5.00 5 -2 -19 -0.50 5.90 -5 2 19 5.00 5.60 5 2 -19 -8.00 4.90 -7 -3 19 -7.90 5.00 7 -3 -19 -14.40 4.90 7 3 -19 0.00 4.90 -7 3 19 0.70 5.10 6 -3 -19 13.30 5.90 -6 -3 19 15.60 5.40 -6 3 19 19.60 6.00 6 3 -19 11.80 5.40 -5 -3 19 28.40 5.80 5 -3 -19 20.90 6.10 5 3 -19 18.40 5.40 -5 3 19 22.00 6.00 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 11484 _publcif_info_exptl_table_max_cols 4 _publcif_info_exptl_table_use_headnotes n loop_ _publcif_info_tables.block_id _publcif_info_tables.reference_item "{d105f0f2-f86b-4b6f-87d0-438749181ddb}" "_publcif_info_datablock.publ_exptl" loop_ _publcif_info_cif.paper_type EE loop_ _publcif_info_datablock.id _publcif_info_datablock.publ_exptl _publcif_info_datablock.publ_geom _publcif_info_datablock.structure '{d105f0f2-f86b-4b6f-87d0-438749181ddb}' y y y loop_ _publcif_info_exptl_table_extra_item sin_theta_over_lambda_max loop_ _publcif_info_exptl_table_header_item ? _publcif_funding_html ; ;